In the ninth century AD, Moravia (now in Czechia) was the heartland of the first Slavic state-like formation in Central Europe. Traditionally, the archaeology of the region has been interpreted via historical records only; the FORMOR project aims to broaden this view by using archaeometry, archaeogenetics, bioarchaeology and introducing new theoretical approaches.

We examine provenance data collected from three types of geological resources recovered at Goat Spring Pueblo in central New Mexico. Our goal is to move beyond simply documenting patterns in compositional data; rather, we develop a narrative that explores how people's knowledge and preferences resulted in culturally and materially determined choices as revealed in those patterns. Our analyses provide evidence that residents of Goat Spring Pueblo did not rely primarily on local geological sources for the creation of their glaze paints or obsidian tools. They did, however, utilize a locally available blue-green mineral for creation of their ornaments. We argue that village artisans structured their use of raw materials at least in part according to multiple craft-specific and community-centered ethnomineralogies that likely constituted the sources of these materials as historically or cosmologically meaningful places through their persistent use. Consequently, the surviving material culture at Goat Spring Pueblo reflects day-to-day beliefs, practices, and social relationships that connected this village to a broader mosaic of interconnected Ancestral Pueblo taskscapes and knowledgescapes.

Minimally invasive compositional analyses of glass trade beads have revolutionised the study of these highly portable and socially significant items. Here, the authors interrogate new and legacy compositional data to investigate how Indigenous communities in eastern North America, particularly Wendat confederacy members, obtained beads from European traders and connected to broader interregional exchange systems c. AD 1600–1670. Diagnostic chemical elements in glass compositions reveal down-the-line exchange and population movement into the Western Great Lakes region prior to the arrival of European settlers, which highlights active Indigenous participation in transatlantic economic networks during a historical period of dynamic reorganisation and interaction.

El objetivo principal de este trabajo es presentar importantes novedades sobre el marco histórico y productivo de la explotación minera de la sierra de Corduba en época romana, así como de la gestión de sus recursos. Desde hace años y a partir de la documentación epigráfica disponible, se ha venido apuntando una posible presencia en este territorio de la societas Sisaponensis y de la explotación de plomo y plata por su parte, a pesar de la afamada vinculación con el beneficio del cinabrio que recoge un conocido pasaje de Plinio. Nuestras investigaciones en el norte de Córdoba y los análisis arqueométricos realizados sobre tres lingotes de plomo recuperados en el paraje de Los Escoriales de Doña Rama, situado en la Sierra de Gata (Belmez-Córdoba), suponen una superación de la frontera del conocimiento sobre los aspectos reseñados, ya que permiten contrastar estas dos hipótesis tradicionales y proponer nuevas cuestiones sobre la explotación de estos parajes y la actividad de esta societas. Estos lingotes fueron encontrados en una instalación minero-metalúrgica romana, algo que es excepcional, y conservan una inscripción, S S, que los vincula sin duda con la societas Sisaponensis.

En este trabajo se presentan los resultados de estudios experimentales realizados en pastas cerámicas con el objetivo de comprender las elecciones técnicas realizadas por los grupos cazadores-recolectores que habitaron el curso inferior del Río Colorado (transición pampeano-patagónica oriental) en los últimos 2000 años aP aproximadamente. A tal efecto, con la guía de ceramistas locales, se realizaron ensayos tanto en el campo como en el laboratorio, empleando materias primas (arcillas y arenas) obtenidas del área de estudio. Durante las tareas de campo se realizó el testeo inicial y la cocción de las materias primas, actividades que se repitieron en el laboratorio. A esto se agregó una batería de estudios arqueométricos (e.g., petrografías, DRX, FTIR, SEM-EDAX) cuyos resultados fueron comparados con la información arqueológica del área. En este sentido, la composición de las materias primas, las temperaturas y condiciones de quema, así como los patrones tecnológicos de las pastas experimentales, son concordantes con las registradas en las cerámicas arqueológicas. La integración de estos datos indicaría la producción preponderantemente local de las vasijas como también la transmisión de una práctica alfarera a lo largo del Holoceno tardío.

With its promise of nondestructive processing, rapid low-cost sampling, and portability to any field site or museum in the world, portable X-ray fluorescence (pXRF) spectrometry is rapidly becoming a standard piece of equipment for archaeologists. Even though the use of pXRF is becoming standard, the publication of pXRF analytical methods and the resulting data remains widely variable. Despite validation studies that demonstrate the importance of sample preparation, data collection settings, and data processing, there remains no standard for how to report pXRF results. In this article, we address the need for best practices in publishing pXRF analyses. We outline information that should be published alongside interpretive results in any archaeological application of pXRF. By publishing this basic information, archaeologists will increase the transparency and replicability of their analyses on an inter-analyst/inter-analyzer basis and provide clarity for journal editors and peer reviewers on publications and grant proposals for studies that use pXRF. The use of these best practices will result in better science in the burgeoning use of pXRF in archaeology.

Este trabajo se propone avanzar en la comprensión de los procesos históricos de pintado del sitio arqueológico de Oyola (Sierra El Alto-Ancasti, Catamarca, Argentina). En particular, se evalúan similitudes y diferencias en la composición material de las mezclas pigmentarias para entrever la existencia de antiguas recetas pictóricas en la confección de las pinturas rupestres negras. Para ello se realizaron análisis microestratigráficos de 28 motivos mediante microscopía electrónica de barrido con análisis elemental por espectroscopía dispersiva en energía de rayos X (MEB-EDS), y microespectroscopía Raman (RS). Su estudio comparativo señaló el uso alternativo de dos pigmentos negros (carbón vegetal y óxidos de manganeso) combinados, en algunos casos, con un aditivo (sulfato de calcio). De esta forma, fue posible conocer ciertos aspectos de las recetas pictóricas que orientaron la preparación de las mezclas pigmentarias negras, aproximándonos a algunas de las tradiciones y saberes retomados. Para alcanzar una comprensión histórica de dichas recetas, se evaluó la distribución espacial, temporal y algunas características formales de los motivos rupestres realizados con ellas. Al no identificarse tendencias claras, se propone una definición menos normativa de receta pictórica que resalta los aspectos compartidos entre distintos episodios de pintado sin perder de vista las posibilidades creativas de cada evento.

Excavations conducted by Beloit College in 1958 and 1960 identified the site of La Magdalena in the Bajío of Mexico. Investigators have since highlighted three primary phases of occupation at La Magdalena, two of which were proposed to have been culturally influenced by Teotihuacan or Tula. Modern research in the Bajío mostly diverges from those postulations of distant connections, supplanting them with local patterns that hold much more explanatory power. Archaeometric studies are pivotal in this regard but have thus far been infrequently used. This research analyzes the obsidian assemblage from La Magdalena and finds a nearly ubiquitous utilization of a local obsidian source known as Ojo Zarco. These findings merit a reevaluation of obsidian in the eastern Bajío and argue for more archaeometric studies that elucidate local procurement patterns.

Glass bangles are found in southern England and Wales from the mid-first century ad and become common in the north of England and southern Scotland in the late first century, before their numbers decline a century later. British bangles develop at a time of change, as Roman glassmaking practices were introduced across large areas of Britain, and as blown, transparent, colourless and naturally-coloured glassware became increasingly popular. In many communities, however, there was still a demand for strongly coloured opaque glass, including for bangles, and glassworkers devised ways of extending their supplies of opaque coloured glass. This study is based on over one hundred and fifty analyses of bangle fragments from sites in Wales, northern England and southern Scotland, spanning this transitional period. The bangle makers recycled coloured glass from imported vessels, and probably beads and bangle-making waste, to supplement supplies of fresh coloured glass. The novel methods used to modify and extend the coloured glass may derive from pre-Roman bead-making industries, and made use of widely available materials, including smithing hammerscale and possibly plant ashes. The results show the shifting balance of indigenous and Roman influences on different bangle types, depending on when and where they were made, and by whom.

This report focuses on the morphometric and elemental analysis of glass beads collected from an adobe structure (CA-SCR-217H-T) at Mission Santa Cruz, which operated between 1791 and the 1830s in the colonial province of Alta (upper) California. Previous chemical research established a chronological framework for opacified beads collected from sites in Canada, the Great Lakes region, and the southeastern United States. Testing the viability of this chronological framework for California, we analyzed 100 white glass beads using a conventional typology and laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS)—the first application of LA-ICP-MS to a California mission. We present the results of the LA-ICP-MS study and then briefly comment on the potential for LA-ICP-MS to refine chronologies associated with colonial missions and other postcontact sites.

Precious ornaments from the Museum Royal Tombs of Sipán were analyzed by X-ray computed microtomography (microCT). The ornaments analyzed were golden earrings produced by the Moche culture that flourished along the north coast of present-day Peru between approximately 100 and 600 AD. Sipán, also known as Huava Rajada, is a mochica archaeological complex in the north of Peru. In particular, the spectacular jewelry, mainly composed of gold, silver, and copper alloys, gilded copper, and tumbaga, from the Museum “Royal Tombs of Sipán,” in Lambayeque, north of Peru, are some of the most sophisticated metalworking ever produced of pre-Columbian America. A portable microCT system consisting of a high-resolution flat panel detector and a mini X-ray tube were used for the structural analysis of these ornaments. The microCT images show parts of the internal structure, highlighting the manufacturing technique and gold sheets joining techniques of the Moche artisans. Furthermore, the advantage of using the portable microCT system for nondestructive testing is clear when the sample cannot be taken to the laboratory.

Early Copper Age pottery sherds discovered in a cave within the crystalline dolomites of the Southern Carpathians (Romania) were investigated by polarized light optical microscopy (OM), X-ray powder diffraction (XRPD) and electron microprobe analysis (EMPA) to obtain information on the pottery production in the Copper Age in the territory of present-day Romania. Microscopically, the clayey matrix of the ceramic body is highly birefringent or consists of low-birefringent and isotropic parts mixed together, containing fragments of quartz, muscovite, alkali feldspar, plagioclase, biotite, chlorite, heavy minerals and metamorphic and magmatic rocks, as well as an opaque material. The EMPA data revealed an Fe-rich illite-like matrix and helped to identify the mineral nature of the inclusions. Local pottery production in bonfires or surface clamps is envisaged. Miocene illitic clays may have been used as raw materials, mixed with a small amount of sandy temper. The thermal changes revealed by OM, the modification of the XRPD peaks and the EMPA data suggest firing temperatures of between 800 and 850°C.

The phenomenon of Iron Age vitrified ramparts has become increasingly recognisable in the last twenty years in the Iberian Peninsula. After the first walls with vitrified stones were discovered in southern Portugal, there have been several findings scattered throughout western Iberia. A chronological sequence from the Late Bronze Age to the Late Iron Age can be established on the basis of the archaeological remains, with reference to different historical and functional conditions. This article reviews the data obtained from the various sites, in order to understand the context in which the stone structures became vitrified. Furthermore, we have analysed samples of stones and mud bricks that have been altered by fire from these sites, which has allowed us to explain the variability in the archaeological record in relation to different historical processes. With all these data, we aim to contribute to our knowledge of a phenomenon that is widespread in Iron Age Europe.

This review aims to consolidate scarce literature on the use of modern nanomechanical testing technique like instrumented nanoindentation in the field of archaeometry materials research. The review showcase on how can the nanoindentation tests provide valuable data about mechanical properties which, in turn, relate to the evolution of ancient biomaterials as well as human history and production methods. This is particularly useful when the testing is limited by confined volumes and small material samples (since the contact size is in the order of few microns). As an emerging novel application, some special considerations are warranted for characterization of archaeometry materials. In this review, potential research areas relating to how nanoindentation is expected to benefit and help improve existing practices in archaeometry are identified. It is expected that these insights will raise awareness for use of nanoindentation at various world heritage sites as well as various museums.

Mineralogical and chemical compositions of residual and sedimentary clays (bulk and <2 μm fraction) from the Nelas region (schist, aplite-pegmatites, granites and Tertiary sediments from both Mondego River margins), Portugal, were studied, aiming to establish indicators for raw materials in ancient ceramic provenance studies. The mineralogy of bulk material does not provide a clear distinction between samples. Among clay minerals, kaolinite dominates, except in the aplite-pegmatites where illite prevails. Smectite was only found in sediments of the left river bank.

A more successful result was the geochemical differentiation of clay types. The weathered schist presents greater enrichment in Cr, whereas the clay fraction of aplite-pegmatites shows enrichment in all the chemical elements studied. The sediments and weathered granites are not easy to differentiate; the best geochemical indicators are U (lower contents in clay-size fraction of sediments) and REE patterns in both bulk and clay-size fraction.

Excavations at several locations in Verteba Cave have uncovered a large amount of human skeletal remains in association with faunal bones and Tripolye material culture. We aim to establish radiocarbon (14C) dates for eight sites and to evaluate whether these deposits are singular events, or slow accumulations over time. 14C measurements, along with stable carbon and nitrogen isotope data from human and faunal remains, were collected from 18 specimens. Stable isotope values were used to evaluate human and animal diet, and whether freshwater reservoir effects offset measured dates. We found diets of the sampled species had limited to no influence from freshwater resources. Human diet appears to be dominated by terrestrial plants and herbivores. Four new sites were identified as Eneolithic. Comparisons of dates from top and bottom strata for two sites (7 and 20) reveal coeval dates, and we suggest that these deposits represent discrete events rather than slow continuous use. Lastly, we identified dates from the Mesolithic (8490±45 BP, 8765±30 BP), Iron Age (2505±20 BP), Slavic state era (1315±25 BP), and Medieval Period (585±15 BP), demonstrating periodic use of the cave by humans prior to and after the Eneolithic.

A solitary unprocessed, 26-cm basalt stone recently found at the Roman (69 AD) site at Kotterbos (Lelystad, the Netherlands), situated 40 km north of the Limes, has been examined petrographically and geochemically. The rock is similar to previously investigated Roman basalt stones and blocks from the Limes in the province of Utrecht. All are alkali olivine basalts and basanites, which are also the dominant rock types in the nearby volcanic hinterland in Germany. On the basis of 23 criteria, including all major and minor elements plus a selection of trace elements, the Kotterbos stone correlates with a distinctive subgroup of Limes basalts. This subgroup is characterised by relatively high Mg# and low TiO2 wt% values, as opposed to the other subgroup with lower Mg# and higher TiO2 wt% values. It is argued that the high Mg#–low TiO2 subgroup and the Kotterbos basalt have common geological provenance(s). Five basalt bodies in the hinterland match the criteria of this subgroup, and might be considered as locations of provenance. Of these five, only Rolandsbogen, located next to an ideal anchorage on the west bank of the Rhine, about 12 km upstream from Bonn, can also conform to sensible Roman demands concerning effective logistics and military safety. Consequently, Rolandsbogen is the most likely site of provenance for the high Mg#–low TiO2 subgroup, which includes the Kotterbos basalt. It is argued that the Kotterbos stone is not a rock that somehow got separated from a shipment of building stones to the northern Limes; rather, it is speculated that the stone was picked up as a stray cobble near the basalt body and taken onboard a Roman vessel moored at the Rolandsbogen anchorage.