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Use of X-Ray Diffraction as an Analytical Technique for the Synthesis of Inorganic Catalysts

Published online by Cambridge University Press:  10 January 2013

G. I. Straguzzi  and
Paden F. Dismore
G. I. Straguzzi*
Affiliation:
Center for Catalytic Science and Technology, Department of Chemical EngineeringUniversity of Delaware, Newark, Delaware 19716
Paden F. Dismore
Affiliation:
Center for Catalytic Science and Technology, Department of Chemical EngineeringUniversity of Delaware, Newark, Delaware 19716
*
*To whom correspondence should be addressed
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Abstract

X-ray powder diffraction was used as an analytical technique for the solid state synthesis of selective oxidation catalysts with large surface area. Qualitative analysis was used to determine the minimum temperature at which the synthesis was complete. Quantitative diffraction was used to analyze mixtures of isomorphous antimonates. Results indicated that the final mixtures are independent of the method of preparation, i.e., mixing or impregnation.

Type
Research Article
Information
Powder Diffraction , Volume 2 , Issue 3 , September 1987 , pp. 183 - 186
Copyright
Copyright © Cambridge University Press 1987

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References

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