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Synthesis of new hybrid material based on copolymer and Pd-nanoparticles.

Published online by Cambridge University Press:  17 December 2012

M. Ugalde ,
E. Chavira ,
M. T. Ochoa-Lara ,
M. A. Canseco ,
E.A. Zaragoza-Contreras ,
C. Quintanar  and
M. Gutiérrez-Nava
M. Ugalde*
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO. Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
E. Chavira
Affiliation:
Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
M. T. Ochoa-Lara
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO.
M. A. Canseco
Affiliation:
Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
E.A. Zaragoza-Contreras
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO.
C. Quintanar
Affiliation:
Facultad de Ciencias, Universidad 3000 Circuito Exterior S/N, C.P. 04510 Ciudad Universitaria, MÉXICO.
M. Gutiérrez-Nava
Affiliation:
CIATEQ A.C., Centro de Tecnología Avanzada, , Carretera México Toluca Km. 53.5, en Fraccionamiento Parque Industrial y Tecnológico, Ex Hacienda Doña Rosa, L. 11, Mz. 3, Toluca, Estado de México, MÉXICO C.P. 52000.
*
*E-mail: [email protected]
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Abstract

In this work, the synthesis of new hybrid material based on a poly (buthyl acrylate –co- vinyl formamide) copolymer using the emulsion polymerization and doped with Pd, is discussed. The copolymer structure was confirmed by FT-IR. Afterwards, Pd nanocrystals previously synthesized, resulting on a spherical shape of ~ 5 nm, as measured by High-resolution transmission electron microscopy (HR-TEM), were deposited on the structure of the organic material. The films were analyzed using AFM and Scanning electron microscopy (SEM), giving rise to a hybrid material that could be applied in areas such as nanolithography, catalysis, and sensors.

Keywords

PolymersensorScanning Electron Microscopy (SEM)
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1483: Symposium S – New Trends in Polymer Chemistry and Characterization , 2012 , imrc12-1483-s5b-p029
Copyright
Copyright © Materials Research Society 2012 

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References

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