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Effect of temperature and strain rate on the mechanisms of indentation deformation of magnesium

Published online by Cambridge University Press:  03 August 2015

M. Haghshenas
Affiliation:
Mechanical & Mechatronics Engineering, University of Waterloo, Waterloo (ON) N2L 3G1, Canada
V. Bhakhri*
Affiliation:
Mechanical & Materials Engineering, the University of Western Ontario, London (ON) N6A 5B9, Canada
R. Oviasuyi
Affiliation:
NOVA Chemical Corporation, Calgary (AB), T2P 5C6, Canada
R.J. Klassen
Affiliation:
Mechanical & Materials Engineering, the University of Western Ontario, London (ON) N6A 5B9, Canada
*
Address all correspondence to V. Bhakhri at[email protected]
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Abstract

Dual-stage, constant loading-rate followed by constant-load, pyramidal indentation experiments were performed to investigate the strain-rate (10−5–10−1/s) and temperature (295–573 K) dependence of pure magnesium. The estimated total activation energy, Q (0.69–1.01 eV), and apparent activation volume, V* (17–28b3), indicate that plastic deformation is controlled by a dislocation cross-slip mechanism. The results from this work and previous studies confirm that, during pyramidal indentation of Mg, the operative deformation mechanism remains the same over a very wide strain-rate and temperature range.

Type
Research Letters
Copyright
Copyright © Materials Research Society 2015 

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References

1.Somekawa, H. and Schuh, C.A.: Nanoindentation behavior and deformed microstructures in coarse-grained magnesium alloys. Scr. Mater. 68, 416419 (2013).Google Scholar
2.Wang, C.L., Mukai, T., and Nieh, T.G.: Room temperature creep of fine-grained pure Mg: a direct comparison between nanoindentation and uniaxial tension. J. Mater. Res. 24, 16151618 (2009).CrossRefGoogle Scholar
3.Sklenička, V., Pahutová, M., Kuchartová, K., Svoboda, M., and Langdon, T.G.: Creep processes in magnesium alloys and their composites. Metall. Mater. Trans. A. 33, 883889 (2002).CrossRefGoogle Scholar
4.Agnew, S.R., Yoo, M.H., and Tomé, C.N.: Application of texture simulation to understanding mechanical behavior of Mg and solid solution alloys containing Li or Y. Acta Mater. 49, 42774289 (2001).Google Scholar
5.Cepeda-Jiménez, C.M., Molina-Aldareguia, J.M., Carreño, F., and Pérez-Prado, M.T.: Prominent role of basal slip during high-temperature deformation of pure Mg polycrystals. Acta Mater. 85, 113 (2015).Google Scholar
6.Somekawa, H. and Schuh, C.A.: High-strain-rate nanoindentation behavior of fine-grained magnesium alloys. J. Mater. Res. 27, 12951302 (2012).Google Scholar
7.Somekawa, H. and Schuh, C.A.: Effect of solid solution elements on nanoindentation hardness, rate dependence, and incipient plasticity in fine grained magnesium alloys. Acta Mater. 59, 75547563 (2011).Google Scholar
8.Catoor, D., Gao, Y.F., Geng, J., Prasad, M.J.N.V., Herbert, E.G., and Kumar, K.S.: Incipient plasticity and deformation mechanisms in single-crystal Mg during spherical nanoindentation. Acta Mater. 61, 29532965 (2013).Google Scholar
9.Ito, K.: The hardness of metals as affected by temperature. Tohoku Sci. Reports 12, 137 (1923).Google Scholar
10.Westbrook, J.H.: Temperature dependence of the hardness of pure metals. Trans. A.S.M. 45, 221 (1953).Google Scholar
11.Bhakhri, V., Wang, J., Ur-rehman, N., Ciurea, C., Giuliani, F., and Vandeperre, L.J.: Instrumented nanoindentation investigation into the mechanical behavior of ceramics at moderately elevated temperatures. J. Mater. Res. 27, 6575 (2012).CrossRefGoogle Scholar
12.Kocks, U.F., Argon, A.S., and Ashby, F.: Thermodynamics and Kinetics of Slip (Pergamon Press, Oxford, 1975).Google Scholar
13.Watanabe, H., Owashi, A., Uesugi, T., Takigawa, Y., and Higashi, K.: Grain boundary relaxation in fine-grained magnesium solid solutions. Philos. Mag. 91, 41584171 (2011).Google Scholar
14.Frost, H.J. and Ashby, F.: Deformation-Mechanism Maps: The Plasticity and Creep of Metals and Ceramics (Pergamon Press, Oxford, 1982).Google Scholar
15.Koike, J., Kobayashi, T., Mukai, T., Watanabe, H., Suzuki, M., and Maruyama, K.: The activity of non-basal slip systems and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys. Acta Mater. 51, 20552065 (2003).Google Scholar
16.Lubarda, V.A., Meyers, M.A., and Vo, O.: The onset of twinning in metals: a constitutive description. Acta Mater. 49, 40254039 (2001).Google Scholar
17.Shih, T.-S. and Liu, Z.-B.: Thermally-formed oxide on aluminum and magnesium. Mater. Trans. 47, 13471353 (2006).Google Scholar
18.Galiyev, A., Kaibyshev, R., and Gottstein, G.: Correlation of plastic deformation and dynamic recrystallization in magnesium alloy ZK60. Acta Mater. 49, 11991207 (2001).Google Scholar
19.Maier, V., Merle, B., Göken, M., and Durst, K.: An improved long-term nanoindentation creep testing approach for studying the local deformation processes in nanocrystalline metals at room and elevated temperatures. J. Mater. Res. 28, 11771188 (2013).Google Scholar
20.Tabor, D.: The Hardness of Metals (Oxford University Press, Oxford, 2000).CrossRefGoogle Scholar