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Directionally solidified Al2O3/ZrO2 eutectic ceramic prepared with induction heating zone melting

Published online by Cambridge University Press:  15 May 2018

Weinan Wang ,
Juncheng Liu  and
Caiyu Song
Weinan Wang
Affiliation:
School of Materials Science and Engineering, Tianjin Polytechnic University, Tianjin 300387, China
Juncheng Liu*
Affiliation:
School of Materials Science and Engineering, Tianjin Polytechnic University, Tianjin 300387, China
Caiyu Song
Affiliation:
School of Materials Science and Engineering, Tianjin Polytechnic University, Tianjin 300387, China
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

To prepare high quality large solidified Al2O3/ZrO2 eutectic ceramic, the preparation processing of the presintered ceramic as a feed rod was investigated via experiments; some parameters of the induction heating zone process were optimized via numerical modeling; an Al2O3/ZrO2 eutectic ceramic rod with a diameter 10 mm was prepared. The results show that increasing the sintering temperature could increase the presintered ceramic’s bulk density, while increasing sintering time had little effect. And the bulk density increased first and then decreased with the molding pressure increase. And the saucer coil obtained a higher temperature gradient than the tubbiness coil for a fixed crucible wall maximum temperature, and the coil turn’s increase could increase the melting zone height in the induction zone melting process. In the directionally solidified Al2O3/ZrO2 eutectic ceramics, Al2O3 phase is the matrix phase, and the ZrO2 phase embedded in the Al2O3 phase mostly with the rod shape, and little with lamellar. The hardness of directionally solidified eutectic ceramics reaches 16.17 GPa and the fracture toughness reaches 4.76 MPa m1/2, which are 1.7 times and 1.5 times of the presintered eutectic ceramic, respectively.

Keywords

Al2O3/ZrO2eutectic ceramicdirectional solidificationinduction heating zone meltingpresintered ceramicssolidified microstructure
Type
Article
Information
Journal of Materials Research , Volume 33 , Issue 11 , 13 June 2018 , pp. 1681 - 1689
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Copyright
Copyright © Materials Research Society 2018 

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References

REFERENCES

Attarian, M. and Taheri, A.K.: Microstructural evolution in creep aged of directionally solidified heat resistant HP-Nb steel alloyed with tungsten and nitrogen. Mater. Sci. Eng., A 659, 104 (2016).Google Scholar
Waku, Y., Nakagawa, N., Wakamoto, T., Ohtsubo, H., Shimizu, K., and Kohtoku, Y.: A ductile ceramic eutectic composite with high strength at 1873 K. Nature 389, 49 (1997).CrossRefGoogle Scholar
Waku, Y., Nakagawa, N., Wakamoto, T., Ohtsubo, H., Shimizu, K., and Kohtoku, Y.: High temperature strength and thermal stability of a unidirectionally solidified eutectic composite. J. Mater. Sci. 33, 1217 (1998).CrossRefGoogle Scholar
Waku, Y., Nakagawa, N., Wakamoto, T., Ohtsubo, H., Shimizu, K., and Kohtoku, Y.: The creep and thermal stability characteristics of a unidirectionally solidified eutectic composite. J. Mater. Sci. 33, 4943 (1998).CrossRefGoogle Scholar
Waku, Y., Sakata, S., Mitani, A., Shimizu, K., and Hasebe, M.: Temperature dependence of flexural strength and microstructure of Al2O3/Y3Al5O12/ZrO2 ternary melt growth composites. J. Mater. Sci. 37, 2975 (2002).Google Scholar
Ma, W., Zhang, J., Su, H., Ren, Q., Yao, B., and Liu, L.: Microstructure transformation from irregular eutectic to complex regular eutectic in directionally solidified Al2O3/GdAlO3/ZrO2 ceramics by laser floating zone melting. J. Eur. Ceram. Soc. 36, 1447 (2015).Google Scholar
Benamara, O., Cherif, M., Duffar, T., and Lebbou, K.: Microstructure and crystallography of Al2O3–Y3Al5O12–ZrO2, ternary eutectic oxide grown by the micro pulling down technique. J. Cryst. Growth 429, 27 (2015).Google Scholar
Liu, G., Wang, Q., Li, J., Chen, Y., and He, B.: Preparation of Al2O3–ZrO2–SiO2, ceramic composites by high-gravity combustion synthesis. Int. J. Refract. Met. Hard Mater. 41, 622 (2013).Google Scholar
Mei, L., Mai, P., Li, J., and Chen, K.: Fabrication of nanostructure Al2O3/ZrO2, (Y2O3) eutectic by combustion synthesis melt-casting under ultra-high gravity. Mater. Lett. 64, 68 (2010).Google Scholar
Fu, H., Guo, J.L., and Liu, L.: Directional Solidification and Processing of Advanced Materials (Science Press, Beijing, 2008).Google Scholar
Lu, B. and Zhang, Y.: Densification behavior and microstructure evolution of hot-pressed SiC–SiBCN ceramics. Ceram. Int. 41, 8541 (2015).Google Scholar
Booth, F., Garrido, L., Aglietti, E., Silva, A., Pena, P., and Baudín, C.: CaZrO3–MgO structural ceramics obtained by reaction sintering of dolomite–zirconia mixtures. J. Eur. Ceram. Soc. 36, 2611 (2016).CrossRefGoogle Scholar
Yang, H., Zhou, X., Yu, J., Wang, H., and Huang, Z.: Effect of microwave sintering time on the flexural properties of the SiC/SiC composites. Ceram. Int. 41, 14692 (2015).CrossRefGoogle Scholar
Jerebtsov, D.A., Mikhailov, G.G., and Sverdina, S.V.: Phase diagram of the system: Al2O3–ZrO2. Ceram. Int. 26, 821 (2000).CrossRefGoogle Scholar
Wang, P., Sun, H.B., Bai, J.H., and Liu, J.C.: Investigation on solid-liquid interface morphology during the A12O3/MgA12O4 eutectic ceramics solidification. J. Synth. Cryst. 40, 1252 (2011).Google Scholar
Mizutani, Y., Yasuda, H., Ohnaka, I., Maeda, N., and Waku, Y.: Coupled growth of unidirectionally solidified Al2O3-YAG eutectic ceramics. J. Cryst. Growth 244, 384 (2002).CrossRefGoogle Scholar
Herring, C.: Effect of change of scale on sintering phenomena. J. Appl. Phys. 21, 301 (1950).CrossRefGoogle Scholar
Balogh, A.G.: Irradiation induced defect formation and phase transition in nanostructured ZrO2. Nucl. Instrum. Methods Phys. Res., Sect. B 282, 48 (2012).CrossRefGoogle Scholar
Berger, M.H. and Sayir, A.: Directional solidification of Al2O3–Al2TiO5 system. J. Eur. Ceram. Soc. 28, 2411 (2008).CrossRefGoogle Scholar
Mesa, M.C., Serrano-Zabaleta, S., Oliete, P.B., and Larrea, A.: Microstructural stability and orientation relationships of directionally solidified Al2O3–Er3Al5O12–ZrO2, eutectic ceramics up to 1600 °C. J. Eur. Ceram. Soc. 34, 2071 (2014).Google Scholar
Khasanov, O., Osipov, V., Dvilis, E., Kachaev, A., Khasanov, A., and Shitov, V.: Nanoscaled grain boundaries and pores, microstructure and mechanical properties of translucent Yb:[LuxY(1−x)O3] ceramics. J. Alloys Compd. 509, S338–S342 (2011).Google Scholar
Ludwig, A. and Leibbrandt, S.: Generalized ‘Jackson–Hunt’ model for eutectic solidification at low and large Peclet numbers and any binary eutectic phase diagram. Mater. Sci. Eng., A S375–377, 540 (2004).CrossRefGoogle Scholar
Akamatsu, S., Bottin-Rousseau, S., and Faivre, G.: Determination of the Jackson–Hunt constants of the In–In2Bi eutectic alloy based on in situ observation of its solidification dynamics. Acta Mater. 59, 7586 (2011).Google Scholar
Stöcker, C. and Ratke, L.: A new ‘Jackson–Hunt’ model for monotectic composite growth. J. Cryst. Growth 203, 582 (1999).Google Scholar
Barin, I. and Platzki, G.: Thermochemical Data of Pure Substances (VCH, Weinheim, 1989).Google Scholar
Gervais, M., Floch, S., Rifflet, J.C., Coutures, J., and Coutures, J.P.: Effect of the melt temperature on the solidification process of liquid garnets Ln3Al5O12 (Ln = Dy, Y, and Lu). J. Am. Ceram. Soc. 75, 3166 (1992).Google Scholar
Zheng, Y., Li, H., Zhou, T., Zhao, J., and Yang, P.: Microstructure and mechanical properties of Al2O3/ZrO2 eutectic ceramic composites prepared by explosion synthesis. J. Alloys Compd. 551, 475 (2013).Google Scholar
Anstis, G.R., Chantikul, P., Lawn, B.R., and Marshall, D.B.: A critical evaluation of indentation techniques for measuring fracture toughness: I, direct crack measurements. J. Am. Ceram. Soc. 64, 533 (1981).Google Scholar
Deng, Y.F., Zhang, J., Su, H.J., Song, K., Liu, L., and Fu, H.Z.: Microstructure and fracture toughness of A12O3/Er3A15O12 eutectic ceramic prepared by laser zone remelting. J. Inorg. Mater. 26, 841 (2011).CrossRefGoogle Scholar
Sayir, A. and Farmer, S.C.: The effect of the microstructure on mechanical properties of directionally solidified Al2O3/ZrO2(Y2O3) eutectic. Acta Mater. 48, 4691 (2000).Google Scholar
Wang, W., Liang, Z., Han, X., Chen, J., Xue, C., and Zhao, H.: Mechanical and thermodynamic properties of ZrO2, under high-pressure phase transition: A first-principles study. J. Alloys Compd. 622, 504 (2015).Google Scholar
Zhai, S.Y., Liu, J.C., and Wang, J.: Microstructure of the directionally solidified ternary eutectic ceramic Al2O3/MgAl2O4/ZrO2. Ceram. Int. 42, 8079 (2016).Google Scholar