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15 - Photoelectron spectrum of NO2

Published online by Cambridge University Press:  05 June 2012

Andrew M. Ellis
Affiliation:
University of Leicester
Miklos Feher
Affiliation:
Neurocrine Biosciences, San Diego
Timothy G. Wright
Affiliation:
University of Nottingham
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Summary

Concepts illustrated: anion photoelectron spectroscopy; electron affinity; vibrational structure and the Franck–Condon principle; link to thermodynamic parameters; molecular orbital information and Walsh diagrams.

The photoelectron spectroscopy of anions is, in many respects, directly analogous to the photoelectron spectroscopy of neutral molecules. However, an important difference is that an electron in the valence shell of an anion is much more weakly bound than in a neutral molecule. In fact there are some molecules, such as N2, that are unable to bind an additional electron at all. The binding energy of an electron in an anion, which is known as the electron affinity (EA), is the energy difference between the neutral molecule and the anion. The electron affinity is defined as a positive quantity if the anion possesses a lower energy than the neutral molecule, i.e. the electron is bound to the molecule and energy must be added to remove it.

The photoelectron spectrum of an anion, also known as the photodetachment spectrum, can provide information on both the anion and the neutral molecule. A good example of this is the photoelectron spectrum of, which was first recorded by Ervin, Ho, and Lineberger [1].

The experiment

The most common method for generating anions in the gas phase is an electrical discharge. Ervin et al. produced by a microwave (ac) discharge through a helium/air mixture. A variety of neutral and charged species would be expected under such conditions, including several possible anions and cations.

Type
Chapter
Information
Electronic and Photoelectron Spectroscopy
Fundamentals and Case Studies
, pp. 129 - 137
Publisher: Cambridge University Press
Print publication year: 2005

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References

Ervin, K. M., Ho, J., and Lineberger, W. C., Journal of Physical Chemistry 92 (1988) 5405CrossRef
Morino, Y., Tanimoto, M., Saito, S., Hirota, E., Awata, R., and Tanaka, T., Journal of Molecular Spectroscopy 98 (1983) 331CrossRef
Lafferty, W. J. and Sams, R. L., Journal of Molecular Spectroscopy 66 (1977) 478CrossRef
Chase, M. W., Davies, C. A., Downey, J. R., Frurip, D. J., McDonald, R. A., and Syverud, A. N., JANAF Thermochemical Tables, 3rd edn., J. Phys. Chem. Ref. Data, Suppl. 14 (1987)
Atomic Energy Levels, C. E. Moore, National Bureau of Standards, Circ. 467, Washington DC, US Department of Commerce, 1949
Hotop, H. and Lineberger, W. C., J. Phys. Chem. Ref. Data 14 (1985) 731CrossRef
A. D. Walsh, J. Chem. Soc. (1953) 2260; ibid. (1953) 2266

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