The radiocarbon dating laboratory at Rice University first became operative in the fall of 1970. A workable technique has been developed although operations are still in a state of flux. The benzene liquid scintillation counting method is used, the benzene being prepared as outlined by Noakes, Kim, and Akers (1967) with the following modifications. The CO2 is further purified prior to storage and measuring by passing it through 3 gas bubblers containing potassium permanganate solution, silver nitrate solution, and a sulfuric acid-sodium dichromate solution (S. Valastro, pers. commun., 1970). Since no C12 C13 analyses are available at present, to insure a complete reaction, both the CO2 generation and the C2H2 generation are continued for ½ hr after all visible signs of reaction have disappeared.