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A Pretreatment Procedure for the AMS Radiocarbon Dating of Sub-Fossil Insect Remains

Published online by Cambridge University Press:  18 July 2016

J A Tripp
Affiliation:
Oxford Radiocarbon Accelerator Unit, Research Laboratory for Archaeology and the History of Art, Oxford University, 6 Keble Road, Oxford OX1 3QJ, England.
T F G Higham
Affiliation:
Oxford Radiocarbon Accelerator Unit, Research Laboratory for Archaeology and the History of Art, Oxford University, 6 Keble Road, Oxford OX1 3QJ, England.
R E M Hedges
Affiliation:
Oxford Radiocarbon Accelerator Unit, Research Laboratory for Archaeology and the History of Art, Oxford University, 6 Keble Road, Oxford OX1 3QJ, England.
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Abstract

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Two pretreatment methods for accelerator mass spectrometry (AMS) dating of insect remains were explored. One method involves a simple acid wash that removes carbonate, while the other is based on the industrial purification of chitin and results in isolation of polymeric chitosan. No contamination is observed from Maillard reactions during the deacetylation reaction used to isolate the chitosan. The methods were tested on Coleoptera samples from two Roman Britain sites. Our results demonstrate that both methods produce acceptable AMS dates that correspond well to the expected age of the deposits from which they came.

Type
Articles
Copyright
Copyright © 2004 by the Arizona Board of Regents on behalf of the University of Arizona 

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