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X-ray powder diffraction data of anilinium trimolybdate tetrahydrate and anilinium trimolybdate dihydrate

Published online by Cambridge University Press:  10 January 2013

A. Rafalska-Łasocha ,
W. Łasocha  and
M. Michalec
A. Rafalska-Łasocha
Affiliation:
Faculty of Chemistry, Jagiellonian University, 30-060 Kraków, ul. Ingardena 3, Poland
W. Łasocha
Affiliation:
Faculty of Chemistry, Jagiellonian University, 30-060 Kraków, ul. Ingardena 3, Poland
M. Michalec
Affiliation:
Faculty of Chemistry, Jagiellonian University, 30-060 Kraków, ul. Ingardena 3, Poland
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Abstract

The X-ray powder diffraction patterns of anilinium trimolybdate tetrahydrate, (C6H5NH3)2Mo3O10·4H2O, and anilinium trimolybdate dihyhydrate, (C6H5NH3)2Mo3O10·2H2O, have been measured in room temperature. The unit cell parameters were refined to a=11.0670(7) Å, b=7.6116(8) Å, c=25.554(3) Å, space group Pnma(62) and a=17.560(2) Å, b=7.5621(6) Å, c=16.284(2) Å, β=108.54(1)°, space group P21(4) or P21/m(11) for orthorhombic anilinium trimolybdate tetrahydrate and monoclinic anilinium trimolybdate dihydrate, respectively.

Type
Research Article
Information
Powder Diffraction , Volume 14 , Issue 4 , December 1999 , pp. 280 - 283
Copyright
Copyright © Cambridge University Press 1999

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References

Appelman, D. E., Evans, H. T, and Handwerker D. S. (1966). “Program X-ray, Geological Survey.”Google Scholar
Łasocha, W., and Hodorowicz, S. (1991). “Preparation and characterization of the anilinum fibrillar isopolymolybdate,” Acta Chim. Hungarica 128, 133–138.Google Scholar
Łasocha, W., Jasnsen, J., and Schenk, H. (1995). “Crystal structure of anilinium trimolybdate,” J. Solid State Chem. 117, 103–107.Google Scholar
Łasocha, W., Janczur, J., and Hodorowicz, S. (1993). “Anilinum molybdates formed in anilinum chloride—molybdenic acid—Water system,” Polish J. Chem. 67, 1024–1034.Google Scholar
Łasocha, W., and Lewinski, K. (1994). “PROSZKI—System of programs for powder diffraction data processing,” J. Appl. Crystallogr. 27, 437–438.Google Scholar
Łasocha, W., and Schenk, H. (1997). “Crystal structure of anilinium pentamolybdate from powder diffraction data. The solution of crystal structure by direct method Package POWSIM”J. Appl. Crystallogr. 30, 909–913.CrossRefGoogle Scholar
Sonneveld, E., and Visser, J. W. (1975). “Automatic collection of powder data from photographs,” J. Appl. Crystallogr. 8, 1–7.Google Scholar
Visser, J. W. (1969). “A fully automatic program for finding the unit cell from powder data,” J. Appl. Crystallogr. 2, 89–95.Google Scholar