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X-ray powder diffraction data for two new compounds (NH4)1.5Ni2V2O7(OH)1.5 · H2O and (NH4)1.5Cu1.125Ni1.125V2O7(OH)2 · H2O

Published online by Cambridge University Press:  06 March 2012

Johana Arboleda  and
Adriana Echavarría
Johana Arboleda
Affiliation:
Grupo Catalizadores y Adsorbentes, Instituto de Química, Universidad de Antioquia, A.A. 1226 – Medellín, Colombia
Adriana Echavarría*
Affiliation:
Grupo Catalizadores y Adsorbentes, Instituto de Química, Universidad de Antioquia, A.A. 1226 – Medellín, Colombia
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
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Abstract

Two new bimetallic and trimetallic compounds (NH4)1.5Ni2V2O7(OH)1.5 · H2O and (NH4)1.5Cu1.125 Ni1.125V2O7(OH)2 · H2O were synthesized by hydrothermal method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and X-Ray fluorescence (XRF). Crystallographic studies showed that both compounds are hexagonal with space group P-62c.

Keywords

cupper nickel vanadatehydrothermal synthesisX-ray diffraction
Type
New Diffraction Data
Information
Powder Diffraction , Volume 26 , Supplement S1 , December 2011 , pp. S51 - S54
Copyright
Copyright © Cambridge University Press 2011

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References

Altamore, A., Camalli, M., Cuocci, C., Giacovazzo, C., Moliterni, A., and Rizzi, R. (2009). “EXPO2009: Structure solution by powder data in direct and reciprocal space,” J. Appl. Crystallogr. 42, 1197–1202.10.1107/S0021889809042915CrossRefGoogle Scholar
Bert, M. W. and Daphne, E. K. (2003). “Chemistry, spectroscopy and the role of supported vanadium oxides in heterogeneous catalysis,” Catal. Today 78, 25–46.10.1016/S0920-5861(02)00323-1Google Scholar
Gamil, A., Nagi, R. E., Samy, M., Turky, A. M., and Hassan, M. A. (2007). “The role of method of preparation of CuO–NiO system on its physicochemical surface and catalytic properties,” Colloids Surf., A 311, 161–169.10.1016/j.colsurfa.2007.06.014Google Scholar
Hoyos, D., Palacio, L. A., Paillaud, J. L., Simon, A., and Guth, J. L. (2004). “[Zn3+xV2−xO7−3x(OH)2+3x] and M[Zn3−xV2O7(OH)2]Cl1−2x.(1 + 2x) H2O two families of zinc vanadates with structures related to the hexagonal structure of [Zn3V2O7(OH)2] · 2H2O,” Solid State Sci. 6, 1251–1258.10.1016/j.solidstatesciences.2004.07.018CrossRefGoogle Scholar
ICDD (2009). Powder Diffraction File, edited by Kabekkodu, S. (International Centre for Diffraction Data, Newtown Square, Pennsylvania).Google Scholar
Laugier, J. and Bochu, B. (2000). LMGP-Suite for Programs for the Interpretation of X-ray Experiments (ENSP/Laboratoire des Materiaux et du Genie Physique, Saint Martin D’ Heres, France).Google Scholar
Stout, G. S. and Jensen, L. H. (1989). A practical Guide for X-ray Structure Determination (John Wiley & Sons, Seattle, Washington).Google Scholar