Hostname: page-component-586b7cd67f-t7czq Total loading time: 0 Render date: 2024-11-23T01:51:05.732Z Has data issue: false hasContentIssue false

X-ray powder diffraction data for meloxicam, C14H13N3O4S2

Published online by Cambridge University Press:  09 April 2014

Xiao Qing Wu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Pei Xiao Tang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Shan Shan Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Li Li Zhang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for meloxicam, C14H13N3O4S2, are reported [a = 6.997(2) Å, b = 8.113(2) Å, c = 13.604(4) Å, α = 85.774(2)°, β = 88.311(1)°, γ = 74.994(1)°, unit-cell volume V = 743.821 Å3, Z = 2, and space group P-1]. All measured lines were indexed, and no detectable impurity was observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2014 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

David, W. I. F., Shankland, K., McCusker, L. B., and Baerlocher, C. (Eds.) (2002). Structure Determination from Powder Diffraction Data (Oxford University Press, Oxford)Google Scholar
Fabiola, G. F., Pattabhi, V., Manjunatha, S. G., Rao, G. V., and Nagarajan, K. (1998). “4-Hydroxy-2-methyl-N-(5-methyl-1,3-thiazol-2-yl)-2H-1, 2-benzothiazine-3-carboxamide 1, 1-dioxide,” Acta Crystallogr. C, 54, 20012003.Google Scholar
Fitzpatrick, C. E., Chapinal, N., Petersson-Wolfe, C. S., DeVries, T. J., Kelton, D. F., Duffield, T. F., and Leslie, K. E. (2013). “The effect of meloxicam on pain sensitivity, rumination time, and clinical signs in dairy cows with endotoxin-induced clinical mastitis,” J. Dairy Sci., 96, 28472856.Google Scholar
Harris, K. D. M. (2012). “Powder diffraction crystallography of molecular solids,” Top. Curr. Chem., 315, 133178.CrossRefGoogle ScholarPubMed
Johnston, L. (2013). “Use of meloxicam for the long-term treatment of musculoskeletal disorders in cats,” U.S. Patent, Appl. no. 20130035330.Google Scholar
Luger, P., Daneck, K., Engel, W., Trummlitz, G., and Wagner, K. (1996). “Structure and physicochemical properties of meloxicam, a new NSAID,” Eur. J. Pharm. Sci., 4, 175187.Google Scholar
Wu, X. Q., Tang, P. X., Pan, Q. Q., Cheng, Q., and Li, H. (2013). “Crystal structure determination of three polycyclic compounds and comparative Rietveld refinement between MS and GSAS programs,” Chin. Sci. Bull., 58, 24302434.Google Scholar