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X-ray powder diffraction data for deoxyschisandrin

Published online by Cambridge University Press:  16 April 2013

Li Li Zhang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Qing Qing Pan
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Dan Xiao
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Xiao Qing Wu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Qing Wang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for deoxyschisandrin, C24H32O6, are reported [a = 13.083(3) Å, b = 19.563(9) Å, c = 8.805(6) Å, β = 90.472(0)°, unit-cell volume V = 2253.82 Å3, Z = 4, and space group P21]. All measured lines were indexed and are consistent with the P21 space group. No detectable impurity was observed.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2013 

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References

Chien, C. F., Wu, Y. T., and Tsai, T. H. (2011). “Biological analysis of herbal medicines used for the treatment of liver diseases,” Biomed. Chromatogr. 25, 2138.CrossRefGoogle ScholarPubMed
Engel, G. E., Wilke, S., König, O., Harris, K. D. M., and Leusen, F. J. J. (1999). “Powder Solve – a complete package for crystal structure solution from powder diffraction patterns,” J. Appl. Crystallogr. 32, 11691179.CrossRefGoogle Scholar
Huang, T. H., Shen, P. N., and Shen, Y. J. (2005). “Preparative separation and purification of deoxyschisandrin andγ-schisandrin from Schisandra chinensis (Turcz.) Baill by high-speed counter-current chromatography,” J. Chromatogr. A 1066, 239242.CrossRefGoogle ScholarPubMed
Ikeya, Y., Taguchi, H., Sasaki, H., Nakajima, K., and Yosioka, I. (1980). “The constituents of Schizandrin chinensis Baill. 13C nuclear magnetic resonance spectroscopy of dibenzocyclooctadience lignans,” Chem. Pharm. Bull. 28, 24142421.CrossRefGoogle Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: powder X-ray diffraction versus single-crystal X-ray diffraction,” Chin. Sci. Bull. 57, 38673871.CrossRefGoogle Scholar
Young, R. A. (1993). The Rietveld Method, IUCr Monographies of Crystallography (Wiley, Oxford).CrossRefGoogle Scholar