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X-ray powder diffraction data for acetamidinium formate C3H8N2O2, elimination of preferred orientation effect

Published online by Cambridge University Press:  26 September 2017

J. Maixner  and
P. Kačer
J. Maixner*
Affiliation:
Central Laboratories, University of Chemistry and Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
P. Kačer
Affiliation:
Department of Organic Technology, University of Chemical Technology Prague, Technická 5, 166 28 Prague, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for acetamidinium formate, C3H8N2O2, are reported [a = 6.4564(5) Å, c = 13.021 (3) Å, unit-cell volume V = 542.8(3) Å3, M.p. = 215(1)°C, ρc = 1.274 g.cm−3, ρm = 1.269 g.cm−3, Z = 4, and space group P43212]. The front-loaded technique got sample with strong preferred orientation because of plate-like shape of crystallites, so the capillary packing was used for final powder data collection. All measured lines were indexed and are consistent with the P43212 space group. No detectable impurities were observed.

Keywords

X-ray powder diffractionacetamidinium formatepreferred orientation
Type
New Diffraction Data
Information
Powder Diffraction , Volume 32 , Issue 4 , December 2017 , pp. 268 - 270
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Copyright
Copyright © International Centre for Diffraction Data 2017 

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