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X-ray powder diffraction data for a new succinylcholine iodide polymorph, 2,2′-[(1,4-dioxobutane-1,4-diyl)bis(oxy)] bis(N,N,N-trimethyl-ethanaminium) iodide

Published online by Cambridge University Press:  05 March 2012

R. Pažout*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Maixner
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Cibulková
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
B. Kratochvíl
Affiliation:
Department of Solid State Chemistry, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for a new succinylcholine iodide polymorph II, C14H30O4N2I2, are reported [a=13.908(3) Å, b=13.184(3) Å, c=11.717(2) Å, β=92.501(3)°, unit-cell volume V=2146,28 Å3, Z=4, space group P21/c]. All measured lines with the exception of one were indexed and are consistent with the P21/c space group. No detectable impurities were observed.

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2011

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References

Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724731. 10.1107/S0021889804014876Google Scholar
De Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108113. 10.1107/S002188986800508XCrossRefGoogle Scholar
Jensen, B. (1970). “The crystal structure of succinylcholine iodide,” Acta Chem. Scand. 24, 25172524. 10.3891/acta.chem.scand.24-2517CrossRefGoogle ScholarPubMed
Smith, G. S. and Snyder, R. L. (1979). “FN: A criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065. 10.1107/S002188987901178XGoogle Scholar