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X-ray powder diffraction data and crystal data of polymorphic form 2 of carnidazole

Published online by Cambridge University Press:  01 March 2012

Hector Novoa de Armas ,
Oswald M. Peeters ,
Norbert Blaton ,
Dirk J. A. De Ridder  and
Henk Schenk
Hector Novoa de Armas*
Affiliation:
Katholieke Universiteit Leuven, Laboratorium voor Analytische Chemie en Medicinale Fysicochemie, Faculteit Farmaceutische Wetenschappen, Van Evenstraat 4, 3000 Leuven, Belgium
Oswald M. Peeters
Affiliation:
Katholieke Universiteit Leuven, Laboratorium voor Analytische Chemie en Medicinale Fysicochemie, Faculteit Farmaceutische Wetenschappen, Van Evenstraat 4, 3000 Leuven, Belgium
Norbert Blaton
Affiliation:
Katholieke Universiteit Leuven, Laboratorium voor Analytische Chemie en Medicinale Fysicochemie, Faculteit Farmaceutische Wetenschappen, Van Evenstraat 4, 3000 Leuven, Belgium
Dirk J. A. De Ridder
Affiliation:
Universiteit van Amsterdam, Laboratorium voor Kristallografie, IMC, Valckenierstraat 65, 1018XE Amsterdam, The Netherlands
Henk Schenk
Affiliation:
Universiteit van Amsterdam, Laboratorium voor Kristallografie, IMC, Valckenierstraat 65, 1018XE Amsterdam, The Netherlands
*
a)Electronic mail: [email protected]
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Abstract

The indexed powder diffraction pattern and related crystallographic data for polymorphic form 2 of carnidazole (C8H12N4O3S) are reported, as a first step in the structure determination by powder diffraction methods. The unit cell dimensions were determined from high resolution synchrotron powder diffraction data (λ=0.079 998 0 nm) and evaluated by indexing programs. The monoclinic cell found for this polymorph is a=1.3908(2) nm, b=08094(2) nm, c=1.0645(2) nm, β=110.82(2)°,V=1.12015(27)nm3, Z=4, Dx=1.445 Mg∕m3.

Keywords

X-ray powder diffractioncarnidazolepolymorphismindexing
Type
New Diffraction Data
Information
Powder Diffraction , Volume 21 , Issue 1 , March 2006 , pp. 56 - 58
Copyright
Copyright © Cambridge University Press 2006

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