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X-Ray Powder Diffraction Analysis of a Photoconductor Material p-Diethylaminobenzaldehyde Diphenylamine Hydrazone

Published online by Cambridge University Press:  10 January 2013

T. C. Huang  and
P. W. Wang
T. C. Huang
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San Jose, CA 95120-6099, U.S.A.
P. W. Wang
Affiliation:
IBM Research Division, Almaden Research Center, 650 Harry Road, San Jose, CA 95120-6099, U.S.A.
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Abstract

A commercially available photoconductor material, p-diethylaminobenzaldehyde diphenylamine hydrazone, C23H25N3, has been purified and recrystallized from an absolute alcohol solution. The triclinic compound has been characterized by X-ray powder diffraction. Experimental 2θ values corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 74 observed reflections with 2θ up to 30.5° are reported. The powder diffraction data have been evaluated, and figures of merit are reported. Unit-cell parameters least-squares refined from the 74 observed reflections of the triclinic compound are in good agreement with those obtained from the single-crystal structure analysis.

Type
Research Article
Information
Powder Diffraction , Volume 4 , Issue 4 , December 1989 , pp. 206 - 208
Copyright
Copyright © Cambridge University Press 1989

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