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X-ray powder diffraction analysis of 2-exo-(β-pyridyl)-6-exo-phenyl-7-oxa-1-azabicyclo[2.2.1]heptane

Published online by Cambridge University Press:  05 March 2012

J. C. Poveda ,
J. A. Henao ,
J. A. Pinilla ,
V. V. Kouznetsov  and
C. Ochoa
J. C. Poveda
Affiliation:
Grupo de Investigacio´n en Quı´mica Estructural, Centro de Investigacio´n en Biomole´culas (CIBIMOL), Escuela de Quı´mica, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
J. A. Henao*
Affiliation:
Grupo de Investigacio´n en Quı´mica Estructural, Centro de Investigacio´n en Biomole´culas (CIBIMOL), Escuela de Quı´mica, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
J. A. Pinilla
Affiliation:
Grupo de Investigacio´n en Quı´mica Estructural, Centro de Investigacio´n en Biomole´culas (CIBIMOL), Escuela de Quı´mica, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
V. V. Kouznetsov
Affiliation:
Laboratorio de Sı´ntesis Orga´nica Fina, Centro de Investigacio´n en Biomole´culas (CIBIMOL), Escuela de Quı´mica, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
C. Ochoa
Affiliation:
Laboratorio de Sı´ntesis Orga´nica Fina, Centro de Investigacio´n en Biomole´culas (CIBIMOL), Escuela de Quı´mica, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
*
a)Author to whom correspondence should be addressed; electronic mail: [email protected]
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Abstract

The X-ray powder diffraction pattern for a bridgehead heterocyclic system was determined. 2-exo-(β-pyridyl)-6-exo-phenyl-7-oxa-1-azabicyclo[2.2.1]heptane, C16H16N2O, is triclinic with refined unit cell parameters a=1.1012(2), b=1.3950(2), c=1.0074(3) nm, α=111.09(2)°, β=104.97(2)°, γ=77.38(2)°, V=1.3813(3) nm3, Z=4, and Dx=1.212 g/cm3 with space group P-1 (No. 2).

Keywords

powder diffraction analysis7-oxa-1-azabicycles
Type
New Diffraction Data
Information
Powder Diffraction , Volume 18 , Issue 1 , March 2003 , pp. 47 - 49
Copyright
Copyright © Cambridge University Press 2003

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