Hostname: page-component-78c5997874-v9fdk Total loading time: 0 Render date: 2024-11-05T16:39:07.160Z Has data issue: false hasContentIssue false
  • English
  • Français

Synthesis and powder X-ray diffraction data of a new iron phosphate Fe(PO4)·0.5H2O

Published online by Cambridge University Press:  10 January 2013

Nubuo Ishizawa ,
Atsushi Saiki ,
Kyoji Ohdan  and
Mamoru Ai
Nubuo Ishizawa
Affiliation:
Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Mirodi-ku, Yokohama 226, Japan
Atsushi Saiki
Affiliation:
Faculty of Engineering, Tokyo Institute of Technology, 2-12-1 Oh-okayama, Meguro-ku, Tokyo 156, Japan
Kyoji Ohdan
Affiliation:
Ube Laboratory, UBE Industries Ltd., 1978-5 Ube 755, Japan
Mamoru Ai
Affiliation:
Department of Applied Chemistry and Biotechnology, Niigata Institute of Technology, 1719 Fujihashi, Kashiwazaki 945-11, Japan
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder-diffraction data were collected for a new iron phosphate, Fe(PO4)·0.5H2O, obtained by reducing FePO4 with oxalic acid at 220 °C in the presence of water vapor and oxygen. The crystal system was determined to be orthorhombic with unit-cell parameters a=15.991(6) Å, b=20.156(7) Å, and c=7.223(2) Å.

Type
Research Article
Information
Powder Diffraction , Volume 13 , Issue 4 , December 1998 , pp. 246 - 248
Copyright
Copyright © Cambridge University Press 1998

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Ai, M., and Ohdan, K. (1997).Applied Catalysis A 165, 461.Google Scholar
Ai, M., Muneyama, E., Kunishige, A., and Ohdan, K. (1994).Bulletin of the Chemical Society of Japan 67, 551.CrossRefGoogle Scholar
Day, R. A. J., and Underwood, A. L. (1980). Quantitative Analysis, 4th ed. (Prentice-Hall, Englewood Cliffs, NJ).Google Scholar
de Wolff, P. M. (1968).J. Appl. Crystallogr. 1,108.CrossRefGoogle Scholar
Hoggins, J. T., Swinnea, J. S., and Steinfink, H. (1983).J. Solid State Chem. 47, 278.Google Scholar
Ijjaali, M., Venturini, G., Gerardin, R., Malaman, B., and Gleitzer, C. (1991).Eur. J. Solid State Inorg. Chem. 28, 983.Google Scholar
Ito, T. (1950). “X-ray Studies on Polymorphism,” Maruzen Co. Ltd., 187.Google Scholar
Ronis, M., and d’Yvoire, F. (1969).C. R. Seances Acad. Sci., Ser. C 269, 1388.Google Scholar
Royen, Von P., and Korinth, J. Z. (1976).Z. Anorg. Chem. 291, 227.Google Scholar
Smith, G. S., and Snyder, R. L. (1979).J. Appl. Crystallogr. 12, 65.Google Scholar
Visser, J. W. (1969).J. Appl. Crystallogr. 2,89.Google Scholar