Hostname: page-component-cd9895bd7-lnqnp Total loading time: 0 Render date: 2024-12-23T19:06:17.787Z Has data issue: false hasContentIssue false

Synthesis and crystallographic data of a new copper phosphate CuPO4H⋅0.5H2O

Published online by Cambridge University Press:  05 March 2012

Germa´n Alberto Sierra
Affiliation:
Department of Chemical Engineering, University of Antioquia, A. A. 1226, Medellı´n, Colombia
Adriana Echavarria Isaza
Affiliation:
Department of Chemical Engineering, University of Antioquia, A. A. 1226, Medellı´n, Colombia
Luz Amparo Palacio*
Affiliation:
Department of Chemical Engineering, University of Antioquia, A. A. 1226, Medellı´n, Colombia
Carlos Saldarriaga
Affiliation:
Department of Chemical Engineering, University of Antioquia, A. A. 1226, Medellı´n, Colombia
*
a)Author to whom correspondence should be addressed; electronic mail: [email protected]

Abstract

A new copper phosphate, CuPO4H⋅0.5H2O, was synthesized using a low temperature hydrothermal method and characterized by powder X-ray diffraction, thermogravimetric analysis, and chemical analysis. The material is monoclinic, space group P21/c, with a=10.6524(2), b=8.4730(2), c=9.2204(2), β=92.43(0), and V=831.47 Å3.

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2003

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Korzenski, M. B., Schimck, G. L., and Kolis, J. W. (1998). “Hydrothermal synthesis and structural determination of the three-dimensional microporous iron (III) phosphate,” Eur. J. Solid State Inorg. Chem. EJSCE5 35, 143160. ess, EJSCE5 CrossRefGoogle Scholar
Laugier, J. and Bochu, B. (2000). “CHECKCELL,” Laboratoire des Mate´riaux et du Ge´nie Physique, Ecole Nationale Supe´rieure de Physique de Grenoble (INPG) Domaine Universitaire BP 46, 38402 Saint Martin d’He´res.Google Scholar
Roisnel, T. and Rodrigez Carvajal, J. (2000). “WINPLOTR,” Laboratoire de Chemie du Solide et Inorganique Moleculaire (UM126511), Universite´ de Rennes 1, 35042 Rennex Cedex, France.Google Scholar
Shirley, R. (1999). The CRYSFIRE System for Automatic Powder Indexing: User’s Manual (The Lattice Press, Surrey, England).Google Scholar
Visser, J. W. (1969). “A fully automatic program for finding the unit cell from powder data,” J. Appl. Crystallogr. JACGAR 2, 8995. acr, JACGAR CrossRefGoogle Scholar
Werner, P. E., Enksson, L., and Wegtdahl, M. (1985). “TREOR, a Semi-Exhaustive Trial and Error Powder Indexing Program for All Symmetries,” J. Appl. Crystallogr. JACGAR 18, 367370. acr, JACGAR CrossRefGoogle Scholar