Hostname: page-component-586b7cd67f-tf8b9 Total loading time: 0 Render date: 2024-11-23T17:31:42.498Z Has data issue: false hasContentIssue false

Synthesis and crystal data for K3Nb3O6Si2O7

Published online by Cambridge University Press:  10 January 2013

S. Launay
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France
P. Mahé
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France
M. Quarton
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France

Abstract

The silicate compound, K3Nb3O6Si2O7, has been synthesized by solid-state reaction. Single crystals were obtained; they crystallized with the hexagonal space group P2c. Refined unit-cell parameters are: a = 9.0377(3), c=8.0465(7)Å, V=569.18(5)Å3, Z=2, Dm = 3.84(4), Dx=3.851. Powder diffraction data are reported.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1994

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Choisnet, J., Nguyen, N., Groult, D., and Raveau, B. (1976). Mat. Res. Bull. 11, 887894.CrossRefGoogle Scholar
Mighell, A. D., Hubbard, C. R., and Stalick, J. K. (1981). NBS*AIDS 80. A FORTRAN Program for Crystallographic Data Evaluation (National Bureau of Standards, Gaithersberg, MD), Tech. Note 1141 (NBS*AIDS 83 is an expanded version of NBS*AIDS 80).CrossRefGoogle Scholar
Pagnoux, C., Guyomard, D., Verbaere, A., Piffard, Y., and Tournoux, M. (1991). C. R. Acad. Sci. Paris 312, Ser. II, 611615.Google Scholar
Pagnoux, C., Verbaere, A., Piffard, Y., and Tournoux, M. (1993). Eur. J. Solid State Inorg. Chem. 30, 111123.Google Scholar
Pagnoux, C. (1993). Thèse de Doctorat, Université de Nantes.Google Scholar
Shannon, R. D. (1976). Acta Cryst., A 32, 751767.CrossRefGoogle Scholar
Smith, G. J., and Snyder, R. L. (1979). J. Appl. Crystallog. 12, 6065.CrossRefGoogle Scholar
Stucky, G. D., Phillips, M. L. R., and Gier, T. E. (1989). Chem. Mater. 1, 492509.CrossRefGoogle Scholar