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Powder diffraction data for methylenedioxymethylamphetamine hydrochloride monohydrate (MDMA.HCl.H2O, Ecstasy hydrate)

Published online by Cambridge University Press:  30 November 2012

D. F. Rendle*
Affiliation:
9 Wiltshire Drive, Wokingham, Berkshire RG40 1TQ, United Kingdom
E. J. Glazier
Affiliation:
9 Wiltshire Drive, Wokingham, Berkshire RG40 1TQ, United Kingdom
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

Powder diffraction data are presented for 3,4-methylenedioxymethylamphetamine hydrochloride monohydrate, the hydrated form of MDMA.HCl, the drug of abuse commonly known as Ecstasy. Samples of pure MDMA.HCl were recrystallized from a variety of solvents, and powder diffraction patterns of the resulting products recorded. Data were collected at room temperature using iron-filtered Co radiation.

Type
New Diffraction Data
Copyright
Copyright © International Centre for Diffraction Data 2012

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References

Boultif, A. and Louer, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Cryst. 37, 724731.CrossRefGoogle Scholar
ICDD (2012). PDF-4/Organics 2012 (Database), edited by Kabekkodu, S. (International Centre for Diffraction Data, Newtown Square, PA, USA).Google Scholar
McMurdie, H. F., Morris, M. C., Evans, E. H., Paretzkin, B., and Wong-Ng, W. (1986). “Methods of producing standard X-ray diffraction patterns,” Powder Diffr. 1, 4043.CrossRefGoogle Scholar
Morimoto, B. H., Lovell, S., and Kahr, B. (1998). “Ecstasy: 3,4-methylenedioxymethylamphetamine (MDMA),” Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 54, 229331.CrossRefGoogle Scholar
Shulgin, A. T. (1986). “The background and chemistry of MDMA,” J. Psychoactive Drugs 18, 291304.CrossRefGoogle ScholarPubMed
Shulgin, A. T. and Shulgin, A. (1992). PiKHaL (Phenethylamines I Have Known and Loved): A Chemical Love Story (Transform Press, Berkeley). (http://www.erowid.org/library/books_online/pihkal/pihkal.shtml) #109 MDMA; MDM; ADAM; Ecstasy; 3,4-methylenedioxy-N-methylamphetamine.Google Scholar
Smith, G. S. and Snyder, R. L. (1979). “F(n): a criterion for rating powder diffraction patterns and evaluating the reliability of powder pattern indexing,” J. Appl. Cryst. 12, 6065.CrossRefGoogle Scholar
Zapata-Torres, G., Cassels, B. K., Parra-Mouchet, J., Mascarenhas, Y. P., Ellena, J., and De Araujo, A. S. (2008). “Quantum-chemical, NMR, and X-ray diffraction studies on (±)-1-[3,4-(methylenedioxy)phenyl]-2-methylaminopropane,” J. Mol. Graph. Model. 26, 12961305.CrossRefGoogle ScholarPubMed
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