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General Expression of Quantitative Phase Analysis for Samples Containing Amorphous Phase

Published online by Cambridge University Press:  10 January 2013

Shao-Dong Wang  and
Xin-Cheng Pu
Shao-Dong Wang
Affiliation:
Building Materials Department, Chongqing Institute of Architecture and Engineering, Chongqing, China
Xin-Cheng Pu
Affiliation:
Building Materials Department, Chongqing Institute of Architecture and Engineering, Chongqing, China
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Abstract

A general expression for the method of QXRPD without standards is given in this paper to solve the problem of phase analysis on samples containing a non-crystalline component. Its application to some specific cases is discussed. The experiments have proved successful in the analysis of cement and sand-lime samples. The technique may also be applicable for the analysis of fly-ash, glass, ceramics, and metals. It is especially convenient in the study of kinetics and mechanism of reactions when the chemical composition of all samples does not change, because it is not necessary to know the mass absorption coefficient of samples. In the mathematical treatment of non-linear equations given in this paper, a method called linearized iteration procedure is first presented by the author.

Type
Research Article
Information
Powder Diffraction , Volume 6 , Issue 2 , June 1991 , pp. 62 - 65
Copyright
Copyright © Cambridge University Press 1991

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References

Garbauskas, M.F. & Goehner, R.P. (1981). Adv. X-ray Anal., 25, 283.Google Scholar
Gou, Changlin (1985). Acta Phisica Sinica, 34, 1451.Google Scholar
Klug, H.P. & Alexander, L.E. (1954). X-ray Diffraction Procedures for Polycrystal and Amorphous Materials, John Wiley, New York.Google Scholar
Renault, J. (1987). Powder Diffraction, 2, 96.CrossRefGoogle Scholar
Starks, T.H., Fang, J.H., & Zevin, L.S. (1984). Mathematical Geology, 76, 351.CrossRefGoogle Scholar
Zevin, L.S. (1977). J. Appl. Crystallogr., 10, 147–150.CrossRefGoogle Scholar