Hostname: page-component-cd9895bd7-mkpzs Total loading time: 0 Render date: 2024-12-24T03:18:12.613Z Has data issue: false hasContentIssue false
  • English
  • Français

Crystal data for [Cu(LIII)XY]·nH2O compounds [LIII=pymep, terpy; X=I, N3; Y=I, NO3, PF6; n=0,1]

Published online by Cambridge University Press:  10 January 2013

M. I. Arriortua ,
M. Insausti ,
R. Cortès  and
J. I. R. Larramendi
M. I. Arriortua
Affiliation:
Departamento de Mineralogía-Petrología, Universidad del Pais Vasco, Aptdo 644, 48080 Bilbao, Spain
M. Insausti
Affiliation:
Departamento de Química Inorgánica, Universidad del Pais Vasco, Aptdo 644
R. Cortès
Affiliation:
Departamento de Química Inorgánica, Universidad del Pais Vasco, Aptdo 644
J. I. R. Larramendi
Affiliation:
Departamento de Química Inorgánica, Universidad del Pais Vasco, Aptdo 644
Get access Rights & Permissions [Opens in a new window]

Abstract

Three new compounds of generalised formula [Cu(LIII)XY]·nH2O [LIII=pymep, terpy; X=I, N3; Y=I, NO3, PF6; n=0,1], pymep (C14H15N3)=N-(6methyl–2-pyridyl–methylene) -2-(2-pyridyl)-ethylamine and terpy (C15H11N3)=2,2′;6′,2″-terpyridine have been prepared by reaction in solution. Crystal data were determined by single-crystal methods. Powder diffraction data and densities determined by a flotation method are also presented.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 3 , September 1994 , pp. 161 - 163
Copyright
Copyright © Cambridge University Press 1994

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Anderson, O. P., Packard, A. B., and Wicholas, M. (1976). Inorg. Chem. 15, 1613–1618.CrossRefGoogle Scholar
Appleman, D. E., and Evans, H. T. Jr., (1973). “Indexing and Least squares refinement of powder diffraction data,” Rep. PB216188. U.S. Dept. of Commerce, NTIS, 5285 Port Royal Rd., Springfield, VA 22151.Google Scholar
Arriortua, M. I., Mesa, J. L., Rojo, T., Debaerdemaeker, T., Beltrán, D., Stratemeier, H., and Reinen, D. (1988). Inorg. Chem. 27, 2976–2981.CrossRefGoogle Scholar
Arriortua, M. I., Vía, J., Larramendi, J. I. R., Díaz, B., Lezama, L., and Rojo, T. (1991). Polyhedron 10, 495–500.CrossRefGoogle Scholar
Larramendi, J. I. R., Díaz, B., Mesa, J. L., Rojo, T., Vía, J., and Arriortua, M. I. (1991). Acta Cryst. C 47, 943–946.CrossRefGoogle Scholar
Laskowsky, E. J., Duggan, D. M., and Hendrickson, D. N. (1975). Inorg. Chem. 14, 2449–2454.CrossRefGoogle Scholar
Nelson, J., and Nelson, M. (1969). J. Chem. Soc. A, 1597–1603.Google Scholar
Norbury, A. H. (1975). Adv. Inorg. Chem. Radiochem. 17, 231–387.CrossRefGoogle Scholar
Rojo, T., Arriortua, M. I., Mesa, J. L., Cortés, R., Villeneuve, G., and Beltrán, D. (1987a). Inorg. Chim. Acta 134, 59–66.CrossRefGoogle Scholar
Rojo, T., Arriortua, M. I., Ruiz, J., Darriet, J., Villenueve, G., and Beltrán, D. (1987b). J. Chem. Soc. Dalton Trans. 285–291.Google Scholar
Rojo, T., Cortés, R., Lezama, L., Mesa, J. L., Vía, J., and Arriortua, M. I. (1989). Inorg. Chim. Acta 165, 91–98.CrossRefGoogle Scholar
Rojo, T., Vlasse, M., and Beltrán, D. (1983). Acta Cryst. C 39, 194–199.Google Scholar