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Crystal Data and Solid-Liquid Transformation Study by DSC of 2 Hydroxymethyl-2 methyl-1,3 propanediol tetrahydrate

Published online by Cambridge University Press:  10 January 2013

M. Laügt ,
M. Teisseire  and
J. Guion
M. Laügt
Affiliation:
Laboratoire de Physique du Solide et Energie Solaire, Pare Sophia Antipolis, rue B. Gregory, 06560 Valbonne, France
M. Teisseire
Affiliation:
Laboratoire de Physique du Solide et Energie Solaire, Pare Sophia Antipolis, rue B. Gregory, 06560 Valbonne, France
J. Guion
Affiliation:
Laboratoire de Chimie Physique, U.F.R. Sciences, Pare Valrose, 06034 Nice, France
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Abstract

2 Hydroxymethyl-2 methyl-1,3 propanediol tetrahydrate has been crystallised from aqueous solutions in the form of transparent tetragonal thin plates. The cell parameters of the unit cell were determined as a = 9.102(1) Å, c = 47.654(6) Å and the space group is I41/ a.

Solid liquid and reverse transformations have been studied by DSC, and a melting enthalpy of 185 kJ.kg−1 at 29.8° C determined.

Type
Research Article
Information
Powder Diffraction , Volume 6 , Issue 4 , December 1991 , pp. 190 - 193
Copyright
Copyright © Cambridge University Press 1991

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