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Crystal and X-Ray Powder Data for a New Organic Diphosphate [NH3(CH2)2NH3]2·P207

Published online by Cambridge University Press:  10 January 2013

Slaheddine Kamoun
Slaheddine Kamoun
Affiliation:
Laboratoire de l'État Solide, École National d'Ingénieurs, 3038 Sfax (Tunisie)
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Abstract

With the help of Boulle's metathesis reaction, we have succeeded in preparing the compound [NH3(CH2)2NH3]2·P207. We describe its chemical preparation and main crystallographic features. The bis(ethylenediammonium) diphosphate salt is monoclinic, space group C2/c, with Z = 4. Unit cell parameters and powder diffraction data for this salt are reported.

Type
Research Article
Information
Powder Diffraction , Volume 6 , Issue 4 , December 1991 , pp. 228 - 230
Copyright
Copyright © Cambridge University Press 1991

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References

Adams, J.M. & Ramdas, V. (1976). Acta Crystallogr. B32, 3224–3227.CrossRefGoogle Scholar
Adams, J.M. & Ramdas, V. (1977). Acta Crystallogr. B33, 3654–3657.CrossRefGoogle Scholar
Boulle, A. (1941). C.R. Acad Sci. (Paris), 206, 517–519.Google Scholar
Calvo, C. (1965). Can. J. Chem. 43, 1147–1153.CrossRefGoogle Scholar
Kamoun, S., Jouini, A. & Daoud, A. (1989). C.R. Acad Sci. (Paris), 308, 923–925.Google Scholar
Kamoun, S., Jouini, A. & Daoud, A. (1990). Acta. Crystallogr. C46, 420–422.Google Scholar
Smith, G.S. & Snyder, R.L. (1979). J. Apply Cryst. 12, 60–65.Google Scholar
Williams, D.E. (1964). USAEC report IS, 1052.Google Scholar