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X-ray powder diffraction pattern for lactitol and lactitol monohydrate

Published online by Cambridge University Press:  10 January 2013

J. Valkonen ,
P. Perkkalainen ,
I. Pitkänen  and
H. Rautiainen
J. Valkonen
Affiliation:
University of Jyväskylä, Department of Chemistry, P.O. Box 35, SF-40351 Jyväskylä, Finland
P. Perkkalainen
Affiliation:
University of Jyväskylä, Department of Chemistry, P.O. Box 35, SF-40351 Jyväskylä, Finland
I. Pitkänen
Affiliation:
University of Jyväskylä, Department of Chemistry, P.O. Box 35, SF-40351 Jyväskylä, Finland
H. Rautiainen
Affiliation:
University of Jyväskylä, Department of Chemistry, P.O. Box 35, SF-40351 Jyväskylä, Finland
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Abstract

Diffraction patterns were recorded, and unit cell dimensions refined by the least-squares method, for lactitol and lactitol monohydrate. Refined unit cell parameters for lactitol are: a =7.622(1) Å, b = 10.764(2) Å, c = 9.375(1) Å, β= 108.25(1)° in space group P21, and those for lactitol monohydrate a =7.844(1) Å, b = 12.673(2) Å, c = 15.942(2) Å in space group P212121.

Keywords

lactitollactitol monohydratepowder diffraction pattern
Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 3 , September 1994 , pp. 213 - 216
Copyright
Copyright © Cambridge University Press 1994

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References

Den Uyl, C. H. (1987). “Technical and commercial aspects of the use of Lactitol in foods as a reduced calorie bulk sweetener,” Dev. Sweeteners 3, 65–81.Google Scholar
Dinnebier, R. E., and Pennartz, P. U. (1993). “ENRAF-GUFI, ein Programmpaket zur Messung und Auswertung von Pulveraufnahmen mit dem 120° 2θ ortsempfindlichen Detektor,” Z. Kristallogr., Suppl. 7, 33–34.Google Scholar
Kanters, J. A., Schouten, A., and van Bommel, M. (1990). “Structure of Lactitol (4-O-β-D-galactopyranosyl-D-glucitol) Monohydrate, an artificial sweetner,” Acta Crystallogr. C 46, 2408–2411.CrossRefGoogle Scholar
Kivikoski, J., Pitkänen, I., and Nurmi, J. (1992a). “Crystal structure of lactitol (4-O-β-D-galactopyranosyl-D-glucitol) trihydrate,” Carbohydr. Res. 232, 189–195.Google Scholar
Kivikoski, J., Pitkänen, I., Valkonen, J., and Heikkilä, H. (1992b). “Crystal structure of lactitol (4-O-β-D-galactopyranosyl-D-glucitol),” Carbohydr. Res. 223, 45–51.CrossRefGoogle ScholarPubMed
Kivikoski, J., Valkonen, J., and Nurmi, J. (1992c). “Crystal structure of lactitol (4-O-β-D-galactopyranosyl-D-glucitol) dihydrate,” Carbohydr. Res. 223, 53–59.CrossRefGoogle ScholarPubMed
Saijonmaa, T., Heikonen, M., Kreula, M., and Linko, P. (1978). “Preparation and characterization of milk sugar alcohol, lactitol,” Milchwissenschaft 33, 733–736.Google Scholar
Smith, G. S., and Snyder, R. L. (1979). “FN: A Criterion for Rating Powder Diffraction Patterns and Evaluating the Reliability of Powder-Pattern Indexing,” J. Appl. Cryst. 12, 60–65.Google Scholar
Werner, P. E. (1969). “A Fortran program for least-squares refinement of crystal structure cell dimensions,” Arkiv för Kemi 31, 513–516.Google Scholar
de Wolff, P. M. (1968). “A Simplified Criterion for Reliability of a Powder Pattern Indexing,” J. Appl. Cryst. 1, 108–113.Google Scholar