Hostname: page-component-78c5997874-fbnjt Total loading time: 0 Render date: 2024-11-05T09:40:29.005Z Has data issue: false hasContentIssue false

X-ray powder diffraction data of 4-N-(4-methylphenyl)amino- 4-(3′-pyridyl)-1-butene

Published online by Cambridge University Press:  06 March 2012

J. C. Poveda
Affiliation:
Grupo de Investigación en Química Estructural, Centro de Investigación en Biomoléculas “CIBIMOL,”Escuela de Química, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
J. A. Henao*
Affiliation:
Grupo de Investigación en Química Estructural, Centro de Investigación en Biomoléculas “CIBIMOL,”Escuela de Química, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
L. Y. Vargas
Affiliation:
Laboratorio de Síntesis Orgánica Fina, Centro de Investigación en Biomoléculas “CIBIMOL,”Escuela de Química, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
V. V. Kouznetsov
Affiliation:
Laboratorio de Síntesis Orgánica Fina, Centro de Investigación en Biomoléculas “CIBIMOL,”Escuela de Química, Facultad de Ciencias, Universidad Industrial de Santander, A. A. 678, Bucaramanga, Colombia
*
a)Author to whom correspondence should be addressed; electronic mail: [email protected]

Abstract

The X-ray powder diffraction pattern for a new precursor in the synthesis of pyridyl tetrahydroquinolines was determined. 4-N-(4-methylphenyl)amine-4-(3′-pyridyl)-1-butene is monoclinic with refined unit cell parameters a=16.554(5), b=7.204(2), c=12.257(3) Å, β=99.76(2)°, V=1440.5(4) Å3, Z=4, and Dx=1.098 g/cm3, with space group P21/n (No. 14).

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2005

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Boultif, A., and Louer, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by succesive dichotomy method,” J. Appl. Crystallogr. JACGAR 24, 987993. acr, JACGAR Google Scholar
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. JACGAR 1, 108113. acr, JACGAR Google Scholar
Dong, C. (1999). “PowderX: Windows-95-based program for powder X-ray diffraction data processing,” J. Appl. Crystallogr. JACGAR 32, 838838. acr, JACGAR Google Scholar
Kouznetsov, V., Urbina, J., Palma, A., López, S., Devia, C., Enriz, D., and Zacchino, S.(2000). “Synthesis and in vitro Antifungal Properties of 4-Aryl-4-N-arylamino-1-butenes and Related Compounds,” Molecules 5, 428–430.Google Scholar
McMurdie, H. F., Morris, M. C., Evans, E. H., Paretzkin, B., and Wong-Ng, W. (1986). “Methods for producing standard X-ray diffraction powder patterns,” Powder Diffr. PODIE2 1, 4043. pdj, PODIE2 Google Scholar
Mighell, A. D., Hubbard, C. R., and Stalick, J. K. (1981). “NBS* AIDS80: A FORTRAN program for crystallographic data evaluation,” National Bureau of Standards (USA), Tech. Note 1141 (NBS* AIDS83 is a development of NBS* AIDS80).Google Scholar
Ochoa, P. C., and Kouznetsov, V. J. (2002). “Recent advancements in the homoallylamine,” J. Heterocycl. Chem. JHTCAD 39, 595. jhd, JHTCAD Google Scholar
Smith, G. S., and Snyder, R. L. (1979). “F(N): A criterion for Rating Powder diffraction Patterns and Evaluating the Reliability of Powder Pattern Indexing,” J. Appl. Crystallogr. JACGAR 12, 6065. acr, JACGAR Google Scholar
Urbina, J. M., Cortés, J. C., Palma, A., López, S. N., Zacchino, S. A., Enriz, D. R., Ribas, J. C., and Kouznetsov, V. V. (2000). “Inhibitors of the Fungal Cell Wall. Synthesis of 4-Aryl-4-N-arylamine-1-butenes and Related Compounds with Inhibitory Activities on β (1–3) Glucan and Chitin Synthases,” Bioorg Med. Chem. BMECEP 8, 691698. 7zp, BMECEP Google Scholar
Vargas, L. Y., Kouznetsov, V., Stashenko, E., Bahsas, A., and Amaro-Luis, J.(2001). “4-N-Aryl(benzyl)amino-4-hetaryl-1-butenes as building blocks in heterocyclic synthesis. New route to 4,6-dimethyl-2-pyridylquinolines from the 4-N-p-methylphenylamino-4-pyridyl-1-butenes,” Heterocycl. Commun. 7, 323–326.Google Scholar
Werner, P. E., Eriksson, L., and Westdahl, M. (1985). “TREOR, a semiexhaustive trial and error powder indexing program for all symmetries,” J. Appl. Crystallogr. JACGAR 18, 367370. acr, JACGAR Google Scholar