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X-ray powder diffraction data for thiamphenicol, C12H15Cl2NO5S

Published online by Cambridge University Press:  17 February 2016

Hong Qin Yang ,
Qing Wang ,
Pei Xiao Tang ,
Bin Tang ,
Ya Ping Li  and
Hui Li
Hong Qin Yang
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
Qing Wang
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
Pei Xiao Tang
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
Bin Tang
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
Ya Ping Li
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for thiamphenicol, C12H15Cl2NO5S, are reported [a = 17.346(3), b = 15.341(0), c = 5.790 (2) Å, α = β = γ = 90°, unit-cell volume V = 1540.8(3) Å3, Z = 4, and space group P212121]. All measured lines were indexed and are consistent with the P212121 space group. No detectable impurities were observed.

Keywords

X-ray powder diffraction datathiamphenicol
Type
Data Reports
Information
Powder Diffraction , Volume 31 , Issue 1 , March 2016 , pp. 80 - 82
Copyright
Copyright © International Centre for Diffraction Data 2016 

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References

Boultif, A. and LoueÈr, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987–993.CrossRefGoogle Scholar
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108–113.Google Scholar
Ghosh, M., Basak, A. K., and Mazumdar, S. K. (1987). “Structure of Thiamphenicol, D-threo-2,2-Dichloro-N-﹛2-hydroxy-1-(hydroxymethyl)-2-[4-(methylsulfonyl) phenyl]ethyl﹜ acetamide,” Acta Crystallogr. C 43, 1552–1555.Google Scholar
Kowalski, P. (2007). “Capillary electrophoretic determination of thiamphenicol in turkeys serum and its pharmacokinetic application,” J. Pharm. Biomed. Anal. 43, 222–227.Google Scholar
Ma, Ch., Chen, H., Sun, N., Ye, Y., and Chen, H. X. (2012). “Preparation of molecularly imprinted polymer monolith with an analogue of thiamphenicol and application to selective solid-phase microextraction,” Food Anal. Methods 5, 1267–1275.Google Scholar
LoueÈr, D. and LoueÈr, M. (1972). “Methode d'essais et erreurs pour l'indexation automatique des diagrammes de poudre,” J. Appl. Crystallogr. 5, 271–275.CrossRefGoogle Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin,” Chin. Sci. Bull. 57, 3867–3871.Google Scholar
Shin, W. and Kim, S. (1983). “The crystal and molecular structure of thiamphenicol,” Bull. Korean Chem. Soc. 4, 79–83.Google Scholar
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 60–65.Google Scholar
Tang, P. X., Wu, X. Q., Zhang, L. L., Cheng, Q., and Li, H. (2013). “X-ray powder diffraction data for norethindrone,” Powder Diffr. (USA). 29, 46–47.Google Scholar
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