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X-ray powder diffraction data for holmium nitrate pentahydrate

Published online by Cambridge University Press:  17 August 2012

J. Maixner  and
V. Bartůněk
J. Maixner*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
V. Bartůněk
Affiliation:
Department of Inorganic Chemistry, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for the holmium nitrate pentahydrate Ho(NO3)3•5H2O are reported [a = 6.642(8) Å, b = 9.55(2) Å, c = 10.56(2) Å, α = 63.672(1)°, β = 84.622(2)°, γ = 76.085(2)°, unit-cell volume V = 582,74 Å3, Z = 2, space group P-1]. Ho(NO3)3•5H2O is isostructural with ytrium nitrate pentahydrate (PDF 01-75-2104) (ICDD, 2011). All measured lines were indexed and are consistent with the P-1 space group. No detectable impurities were observed.

Keywords

X-ray powder diffractionholmium nitrate pentahydrate
Type
New Diffraction Data
Information
Powder Diffraction , Volume 27 , Issue 3 , September 2012 , pp. 203 - 207
Copyright
Copyright © International Centre for Diffraction Data 2012

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References

Balboul, B. (2000). “Physicochemical characterization of the decomposition course of hydrated holmium nitrate. Thermoanalytical studies,” Powder Technol. 107(1–2), 168–174.CrossRefGoogle Scholar
Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724–731.CrossRefGoogle Scholar
de Wollf, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108–113.CrossRefGoogle Scholar
Farok, H. M., Saunders, G. A., Lambson, W. A., Kruger, R., Senin, H. B., Bartlett, S., and Takel, S. (1996). “An ‘Alexandrite’ effect and optical properties of holmium metaphosphate glass,” Phys. Chem. Glasses 37(3), 125–128.Google Scholar
Fox, R. V., Ball, R. D., Harrington, P. D., Rollins, H. W., and Wai, C. M. (2005). “Holmium nitrate complexation with tri-n-butyl phosphate in supercritical carbon dioxide,” J. Supercrit. Fluids 36(2), 137–144.CrossRefGoogle Scholar
Helfand, B. T., Manvar, A. M., Auffenberg, G. B., Blackwell, R., Hartman, R. J., and McVary, K. T. (2010). “Holmium laser ablation and enucleation of the prostate: a pilot study of the hybrid technique,” Can. J. Urol. 17(3), 5190–5194.Google ScholarPubMed
ICDD (2011). Powder Diffraction File, edited by McClune, Frank (International Centre for Diffraction Data, Newtown Square, PA USA)Google Scholar
Macdonald, R. P. (1964). “Uses for holmium oxide filter in spectrometry,” Clin. Chem. 10(12), 1117.CrossRefGoogle Scholar
Norek, M. and Peters, J. A. (2011). “MRI contrast agents based on dysprosium or holmium,” Prog. Nucl. Magn. Reson. Spectrosc. 59(1), 64–82.CrossRefGoogle ScholarPubMed
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar
Suardi, N., Gallina, A., Salonia, A., Briganti, A., Deho, F., Zanni, G., Abdollah, F., Naspro, R., Cestari, A., Guazzoni, G., Rigatti, P., and Montorsi, F. (2009). “Holmium laser enucleation of the prostate and holmium laser ablation of the prostate: indications and outcome,” Curr. Opin. Urol. 19(1), 38–43.CrossRefGoogle ScholarPubMed
Travis, J. C., Zwinkels, J. C., Mercader, F., Ruiz, A., Early, E. A., Smith, M. V., Noel, M., Maley, M., Kramer, G. W., Eckerle, K. L., and Duewer, D.L. (2002). “An international evaluation of holmium oxide solution reference materials for wavelength calibration in molecular absorption spectrophotometry,” Anal. Chem. 74(14), 3408–3415.CrossRefGoogle ScholarPubMed
Yan, B. and Chen, Z. (2001). “Cyano-bridged aqua(N,N-dimethylacetamide)(cyanoiron) lanthanides from samarium, gadolinium, or holmium nitrate and potassium hexacyanoferrate: crystal structures and magnetochemistry,” Helv. Chim. Acta 84(4), 817–829.3.0.CO;2-U>CrossRefGoogle Scholar