Hostname: page-component-78c5997874-94fs2 Total loading time: 0 Render date: 2024-11-06T01:15:06.532Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction data for a new succinylcholine iodide polymorph, 2,2′-[(1,4-dioxobutane-1,4-diyl)bis(oxy)] bis(N,N,N-trimethyl-ethanaminium) iodide

Published online by Cambridge University Press:  05 March 2012

R. Pažout ,
J. Maixner ,
J. Cibulková  and
B. Kratochvíl
R. Pažout*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Maixner
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Cibulková
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
B. Kratochvíl
Affiliation:
Department of Solid State Chemistry, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for a new succinylcholine iodide polymorph II, C14H30O4N2I2, are reported [a=13.908(3) Å, b=13.184(3) Å, c=11.717(2) Å, β=92.501(3)°, unit-cell volume V=2146,28 Å3, Z=4, space group P21/c]. All measured lines with the exception of one were indexed and are consistent with the P21/c space group. No detectable impurities were observed.

Keywords

X-ray powder diffractioncrystal structuresuccinylcholine iodide
Type
New Diffraction Data
Information
Powder Diffraction , Volume 26 , Issue 3 , September 2011 , pp. 280 - 282
Copyright
Copyright © Cambridge University Press 2011

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724–731. 10.1107/S0021889804014876Google Scholar
De Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108–113. 10.1107/S002188986800508XCrossRefGoogle Scholar
Jensen, B. (1970). “The crystal structure of succinylcholine iodide,” Acta Chem. Scand. 24, 2517–2524. 10.3891/acta.chem.scand.24-2517CrossRefGoogle ScholarPubMed
Smith, G. S. and Snyder, R. L. (1979). “FN: A criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 60–65. 10.1107/S002188987901178XGoogle Scholar