Hostname: page-component-586b7cd67f-t7czq Total loading time: 0 Render date: 2024-11-29T15:19:31.976Z Has data issue: false hasContentIssue false
  • English
  • Français

X-Ray Powder Data for Tetracycline-urea Tetrahydrate, C23H36N4O13 and Tetracycline Hexahydrate, C22H24N2O8·6H2O

Published online by Cambridge University Press:  10 January 2013

Frank N. Blanchard  and
Gus J. Palenik
Frank N. Blanchard
Affiliation:
Department of Geology and Department of ChemistryUniversity of Florida, Gainesville, Florida 32611, U.S.A.
Gus J. Palenik
Affiliation:
Department of Geology and Department of ChemistryUniversity of Florida, Gainesville, Florida 32611, U.S.A.
Get access Rights & Permissions [Opens in a new window]

Abstract

Indexed powder diffraction patterns and related crystallographic data are reported for tetracycline-urea tetrahydrate and tetracycline hexahydrate, neither of which is represented in the X-ray Powder Diffraction File. Objective evaluation of the data indicates high precision of d-spacings and unit-cell parameters, intensities that are acceptably reproducible, sensitivity for low intensity reflections, good resolution of closely spaced reflections, and close correspondence with calculated patterns.

Type
Research Article
Information
Powder Diffraction , Volume 4 , Issue 3 , September 1989 , pp. 168 - 171
Copyright
Copyright © Cambridge University Press 1989

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Appleman, D.E. & Evans, H.T. Jr., (1967). Geol. Soc. Amer. Spec. Pap. 115 (abstract).Google Scholar
Appleman, D.E. & Evans, H.T. Jr., (1973). Report PB216188, U.S. Dept. of Commerce, National Technical Information Service, 5285 Port Royal Rd., Springfield, VA 22151.Google Scholar
Blanchard, F.N. (in press). Pow. Diff.Google Scholar
Blanchard, F.N. & Palenik, G.J. (1989). Pow. Diff. 4, 21–24CrossRefGoogle Scholar
Blanchard, F.N. & Saligan, P.P. (1989). Pow Diff. 4, 26–28CrossRefGoogle Scholar
Blanchard, F.N. (1986). In Adv. X-ray Anal. 29, 225–233. New York: Plenum.Google Scholar
Garvey, R.G. (1986). Pow. Diff. 1, 114.Google Scholar
Garvey, R.G. (1988). A PC version of the program NBS*AIDS83. Annual meeting of the International Centre for Diffraction Data, March 17, 1988, Wilmington, DE.Google Scholar
Hubbard, C.R. (1982). Fluorophlogopite-Low 2θ/Large D-spacing Powder Diffraction Standard Reference Material 675. Obtainable from the National Institute of Standards and Technology, Office of Standard Reference Materials, Gaithersburg, MD 20899.Google Scholar
Hubbard, C.R., Robbins, C. & Wong-Ng, W. (1987). Standard Reference Material 640b, Silicon Powder X-Ray Diffraction Standard. Obtainable from the National Institute of Standards and Technology, Office of Standard Reference Materials, Gaithersburg, MD 20899.Google Scholar
Mitscher, L.A. (1978). The chemistry of the tetracycline antibiotics. Medicinal Research 9. New York: Marcel Dekker.Google Scholar
NBS*AIDS83 (1987). A manual describing the data format used in NBS*AIDS83. Swarthmore: International Centre for Diffraction Data.Google Scholar
Palenik, G. J. & Bentley, J.A. (1978) J. Am. Chem. Soc., 100, 2863–2867.CrossRefGoogle Scholar
Palenik, G.J. & Mathew, M. (1978). J. Am. Chem. Soc., 100, 4464–4469.CrossRefGoogle Scholar
Palenik, G.J., Mathew, M. & Restivo, R. (1978). J. Am. Chem. Soc., 100, 4458–4464.CrossRefGoogle Scholar
Smith, D.K., Nichols, M.C., & Zolensky, M.E. (1983). A FORTRAN IV program for calculating X-ray powder diffraction patterns - Version 10, 72 pp. The Pennsylvania State University, University Park, PA.Google Scholar
Smith, D. K. & Smith, K.L. (1987). Materials Data Inc., Livermore, CA.Google Scholar
Smith, G.S. & Snyder, R.L. (1979). J. Appl. Crystallogr., 12, 60–65.CrossRefGoogle Scholar
Stezowski, J. J. (1976). J. Am. Chem. Soc., 98, 6012–6018.CrossRefGoogle Scholar