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Synthesis and powder X-ray diffraction data of a new iron phosphate Fe(PO4)·0.5H2O

Published online by Cambridge University Press:  10 January 2013

Nubuo Ishizawa ,
Atsushi Saiki ,
Kyoji Ohdan  and
Mamoru Ai
Nubuo Ishizawa
Affiliation:
Materials and Structures Laboratory, Tokyo Institute of Technology, 4259 Nagatsuta, Mirodi-ku, Yokohama 226, Japan
Atsushi Saiki
Affiliation:
Faculty of Engineering, Tokyo Institute of Technology, 2-12-1 Oh-okayama, Meguro-ku, Tokyo 156, Japan
Kyoji Ohdan
Affiliation:
Ube Laboratory, UBE Industries Ltd., 1978-5 Ube 755, Japan
Mamoru Ai
Affiliation:
Department of Applied Chemistry and Biotechnology, Niigata Institute of Technology, 1719 Fujihashi, Kashiwazaki 945-11, Japan
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Abstract

X-ray powder-diffraction data were collected for a new iron phosphate, Fe(PO4)·0.5H2O, obtained by reducing FePO4 with oxalic acid at 220 °C in the presence of water vapor and oxygen. The crystal system was determined to be orthorhombic with unit-cell parameters a=15.991(6) Å, b=20.156(7) Å, and c=7.223(2) Å.

Type
Research Article
Information
Powder Diffraction , Volume 13 , Issue 4 , December 1998 , pp. 246 - 248
Copyright
Copyright © Cambridge University Press 1998

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