Hostname: page-component-cd9895bd7-hc48f Total loading time: 0 Render date: 2024-12-25T13:43:24.142Z Has data issue: false hasContentIssue false
  • English
  • Français

Powder X-ray diffraction data for Ba4ZnTi11O27 and Ba2ZnTi5O13

Published online by Cambridge University Press:  10 January 2013

C. G. Lindsay ,
C. J. Rawn  and
R. S. Roth
C. G. Lindsay
Affiliation:
NIST, Materials Building 223, A215, Gaithersburg, Maryland 20899
C. J. Rawn
Affiliation:
NIST, Materials Building 223, A215, Gaithersburg, Maryland 20899
R. S. Roth
Affiliation:
NIST, Materials Building 223, A215, Gaithersburg, Maryland 20899
Get access Rights & Permissions [Opens in a new window]

Abstract

Single crystals and powder samples of Ba4ZnTi11O27 and Ba2ZnTi5O13 have been synthesized and studied using single-crystal X-ray precession photographs and X-ray powder diffraction. Unit cell dimensions were calculated from a least-squares refinement with a final maximum Δ2θ of 0.05°. Both phases were found to have monoclinic cells, space group C2/m. The refined lattice parameters for the Ba4ZnTi11O27 compound are a= 19.8687(8) Å, b=11.4674(5) Å, c=9.9184(4) Å, β= 109.223(4)°, and Z=4. The refined lattice parameters for the Ba2ZnTi5O13 compound are a= 15.2822(7) Å, b=3.8977(1) Å, c=9.1398(3) Å, β=98.769(4)°, and Z=2.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 1 , March 1994 , pp. 56 - 62
Copyright
Copyright © Cambridge University Press 1994

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Roth, R. S., Rawn, C. J., Lindsay, C. G., and Wong-Ng, W. (1992). Submitted to J. Solid State Chem.Google Scholar
Schmachtel, J., and Müller-Buschbaum, H. (1981). Z. anorg. allg. Chem. 472, 89–94.CrossRefGoogle Scholar
Smith, D. K., Nichols, M. C., and Zolensky, M. E. (1983). POWD10: A FORTRAN IV program for calculating X-ray Powder Diffraction Patterns—version 10 (Department of Geosciences, The Pennsylvania State University, University Park, PA).Google Scholar