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Powder X-ray characterization of lithium thiazolidine-4-carboxylate

Published online by Cambridge University Press:  29 February 2012

S. G. Antonio ,
C. O. Paiva-Santos ,
P. P. Corbi ,
A. C. Massabni  and
F. C. Andrade
S. G. Antonio
Affiliation:
Departamento de Físico-Química, Instituto de Química-UNESP, Caixa Postal 355, CEP 14801-970, Rua Prof. Francisco Degni, s/n, Araraquara, SP, Brazil
C. O. Paiva-Santos
Affiliation:
Departamento de Físico-Química, Instituto de Química-UNESP, Caixa Postal 355, CEP 14801-970, Rua Prof. Francisco Degni, s/n, Araraquara, SP, Brazil
P. P. Corbi*
Affiliation:
Departamento de Ciências Biológicas e da Saúde, Centro Universitário de Araraquara-UNIARA, Associação São Bento de Ensino. Rua Voluntários da Pátria, 1309, CEP 14801-320, Araraquara, SP, Brazil
A. C. Massabni
Affiliation:
Departamento de Química Geral e Inorgânica, Instituto de Química-UNESP, Caixa Postal 355, CEP 14801-970, Rua Prof. Francisco Degni, s/n, Araraquara, SP, Brazil
F. C. Andrade
Affiliation:
Departamento de Química Geral e Inorgânica, Instituto de Química-UNESP, Caixa Postal 355, CEP 14801-970, Rua Prof. Francisco Degni, s/n, Araraquara, SP, Brazil
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected] or [email protected]
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Abstract

Powder X-ray diffraction studies of a lithium salt of thiazolidine-4-carboxylic acid (Li-TC4) of composition LiC4H6NSO2 are presented in this paper. Analysis of the synchrotron powder X-ray diffraction data showed that the complex has an orthorhombic symmetry with space group P212121. Unit cell parameters after the refinement using the Pawley method are: a=19.4931(3) Å, b=4.947 77(6) Å, c=6.201 64(8) Å, and V=598.051 Å3.

Keywords

X-raypowder diffractionamino acidsthiazolidine-4-carboxylic acid
Type
New Diffraction Data
Information
Powder Diffraction , Volume 24 , Issue 1 , March 2009 , pp. 44 - 47
Copyright
Copyright © Cambridge University Press 2009

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