Hostname: page-component-586b7cd67f-t7fkt Total loading time: 0 Render date: 2024-11-26T04:21:20.916Z Has data issue: false hasContentIssue false

Powder Diffraction Data for Two Bivalent Metal Hydroxide Nitrates Cd5(OH)8(NO3)2·2H2O and Zn5(OH)8(NO3)2·2NH3

Published online by Cambridge University Press:  10 January 2013

Patricia Bénard
Affiliation:
Laboratoire de Cristallochimie (URA 254), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes cedex, France.
Daniel Louër
Affiliation:
Laboratoire de Cristallochimie (URA 254), Université de Rennes I, Avenue du Général Leclerc, 35042 Rennes cedex, France.

Abstract

Cadmium hydroxide nitrate dihydrate, Cd5(OH)8(NO3)2·2H2O, and zinc hydroxide nitrate diammoniac, Zn5(OH)8(NO3)2·2NH3, have been investigated by means of X-ray powder diffraction. Their unit cell dimensions were found by an indexing program and confirmed by single crystal studies. Precise data collected with strictly monochromatic radiation are reported. The figures of merit are F30=118 (0.0071,36) for the cadmium compound and F30=53 (0.015,38) for the zinc compound. A short discussion of the unit cell parameters compared to those of a related zinc hydroxide nitrate dihydrate is presented.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1990

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Auffrédic, J.P., Plévert, J.& Louër, D.(1990). J. Solid State Chem. 84, 5870.Google Scholar
Bénard, P., Louër, M., Auffrédic, J.P.& Louër, D.(1990). To be published.Google Scholar
de Haan, Y.M.(1963). Nature (London) 200, 876.Google Scholar
Louër, D., Auffrédic, J.P., Langford, J.I., Ciosmak, D.& Niepce, J.C.(1983). J. Appl. Crystallogr. 16, 183191.Google Scholar
Louër, D.& Langford, J.I.(1988). J. Appl. Crystallogr. 21, 430437.Google Scholar
Louër, D., Mesnier, M.T.& Niepce, J.C.(1984). J. Mater. Sci. 19, 716722.Google Scholar
Louër, D.& Vargas, R.(1982). J. Appl. Crystallogr. 15, 542545.Google Scholar
Mighell, A.D., Hubbard, C.R.& Stalick, J.K.(1981). NBS*AIDS80: A FORTRAN program for Crystallographic Data Evaluation. NBS (U.S.) Tech. Note 1141. (NBS*AIDS83 is an expanded version of NBS*AIDS80).Google Scholar
Stählin, W.& Oswald, H.R.(1970). Acta Crystallogr. B26, 860863.Google Scholar