Hostname: page-component-586b7cd67f-t8hqh Total loading time: 0 Render date: 2024-11-26T02:03:57.839Z Has data issue: false hasContentIssue false
  • English
  • Français

High Quality Powder Diffraction Data from an Impure Specimen: Triphylite, Li(Fe,Mn)PO4

Published online by Cambridge University Press:  10 January 2013

Frank N. Blanchard  and
Pablo P. Saligan
Frank N. Blanchard
Affiliation:
University of Florida, Gainesville, Florida 32611, U.S.A. and the Philippine Atomic Energy Commission, Manila, Philippines
Pablo P. Saligan
Affiliation:
University of Florida, Gainesville, Florida 32611, U.S.A. and the Philippine Atomic Energy Commission, Manila, Philippines
Get access Rights & Permissions [Opens in a new window]

Abstract

High quality powder diffraction data were obtained from a specimen containing inseparable impurities, by using single crystal precession photographs to explore all possible reflections for the mineral being studied. In this manner it is acceptable to ignore weak reflections that do not index on the unit cell and that are not observed on the single crystal photographs. Triphylite is given as an example.

Type
Research Article
Information
Powder Diffraction , Volume 4 , Issue 1 , March 1989 , pp. 26 - 28
Copyright
Copyright © Cambridge University Press 1989

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Appleman, D. E. & Evans, H. T. Jr., (1973). Report PB216188, U. S. Dept. of Commerce, National Technical Information Service, 5285 Port Royal Rd., Springfield, VA 22151.Google Scholar
Blanchard, F. N. (1985). In Adv. X-ray Anal. 28, 305–308. New York: Plenum.Google Scholar
Garvey, R. G. (1986). Pow. Diff. 1, 114.Google Scholar
Garvey, R. G. (1988). Annual meeting of the International Centre for Diffraction Data, March 17, 1988, Wilmington, DE.Google Scholar
Geller, S. & Durand, J. L. (1960). Acta Crystallogr. 13, 325–331.CrossRefGoogle Scholar
MPDF, Mineral Powder Diffraction File (1986). Swarthmore, PA: International Centre for Diffraction Data.Google Scholar
NBS* AIDS83 (1987). Swarthmore, PA: International Centre for Diffraction Data.Google Scholar
Smith, D. K., Nichols, M. C. & Zolensky, M. E. (1983). A FORTRAN IV program for calculating X-ray powder diffraction patterns - Version 10, 72 pp. The Pennsylvania State University, University Park, PA.Google Scholar
Smith, D. K. & Smith, K. L. (1987). Materials Data Inc., Livermore, CA.Google Scholar
Yakubovich, O. V., Simonov, M. A. & Belov, N. V. (1977). Sov. Phys. Dokl. 22, 347–348.Google Scholar