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Tm Analysis of Interfaces Beiween Nb and Al2O3 Precipitates

Published online by Cambridge University Press:  26 February 2011

W. Mader*
Affiliation:
Max—Planck—Institut für Metallforzchung, Institut für Werkstoffwissenschaften, Seestrasse 92, 7000 Stuttgart 1, Federal Republic of Germany
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Abstract

A Nb—Al alloy has been internally oxidized to produce A12O3precipitates. The interface between plate—like AI2O3 precipitates and the Nb matrix has been investigated by diffraction, CTEM, and HREM techniques. Periodic arrays of misfit dislocations were observed which acted as diffraction gratings for the electrons. The location of misfit dislocation cores could be determined from HREM images within an accuracy of a few lattice spacings. It can be concluded that the misfit dislocations lead to a good matching of atomic rows across the interface. The dislocation arrangement at this partially coherent interface is in accordance with theoretical expectations from dislocation theory.

Type
Research Article
Copyright
Copyright © Materials Research Society 1987

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References

REFERENCES

[1] Gibson, J.M. and Dawson, L.R. (eds.), Layered Structures, Epitaxy and Interfaces, MRS Syop. Proc. Vol. 37 (Materials Research Society, Pittsburgh, 1985).Google Scholar
[2] Giess, E.A., Tu, K.-N., and Uhlmann, D.R. (eds.), Electronic Packaging Materials Science, MRS Syrup. Proc., Vol. 40 (Materials Research Society, Pittsburgh, 1985).Google Scholar
[3] Rihle, M., Balluffi, R. W., Fischmeister, H., and Sass, S.L. (eds.), Int. Conf. on the Structure and Properties of Internal Interfaces, J. de Physique, Colloque C4 (1985).Google Scholar
Turwitt, M., Elssner, G., and Petzow, G., ibid., pp. 123127.Google Scholar
Florjancic, M., Mader, W., Ruhle, M., and Turwitt, M., ibid., pp. 129133.Google Scholar
[4] Burger, K., Mader, W., and Ruhle, M., Ultramicroscopy (in the press).Google Scholar
[5] Rihle, M., Backhaus-Ricoult, M., Burger, K., and Mader, W., Conf. on Ceraic Microstructures '86: Role of Interfaces, University of California, 1986 (to be published).Google Scholar
[6] Doychak, J.K., Eastman, J.A., and Mader, W., (unpublished).Google Scholar
[7] Ashby, M.F. and Smith, G.C., J. Inst. Metals 91, 182 (1963).Google Scholar
[8] Matthews, J.W., in Dislocations in Solids, Vol. 2, edited by Nabarro, F.R.N. (North-Holland, Amsterdam, New York, Oxford, 1979) pp. 461545.Google Scholar
[9] Johnson, K.H. and Pepper, S.V., J. Appl. Phys. 53, 6634 (1982).Google Scholar