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Template-Assisted Fabrication of Double-Shelled Nanotubes Composed of Inner Shell Pb(Zr0.52Ti0.48)O3 and Outer Shell TiO2 by Sol-Gel Process with Spin-Coating Technique

Published online by Cambridge University Press:  14 March 2011

Y. C. Choi
Affiliation:
Department of Physics, Chonbuk National University, Jeonju 561-756, Korea
S. Y. Cho
Affiliation:
Department of Physics, Chonbuk National University, Jeonju 561-756, Korea
S. D. Bu*
Affiliation:
Department of Physics, Chonbuk National University, Jeonju 561-756, Korea
*
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Abstract

Double-shelled nanotubes composed of inner shell Pb(Zr0.52Ti0.48)O3 (PZT) and outer shell TiO2 are successfully fabricated by a spin coating of each sol-gel solution on porous anodic alumina template. Field emission transmission electron microscopy images show that they have a ~ 10 nm wall thickness. The selected area electron diffraction patterns show that they have two mixed crystalline phases of tetragonal PZT and anatase TiO2. The analyses of scanning transmission electron microscopy equipped with energy dispersive X-ray spectroscopy confirm their uniform distribution of each element.

Type
Research Article
Copyright
Copyright © Materials Research Society 2011

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