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Synthesis of AlFe Intermetallic Nanoparticles by High-Energy Ball Milling

Published online by Cambridge University Press:  12 May 2015

G. Rosas ,
J. Chihuaque ,
E. Bedolla ,
R. Esparza  and
R. Pérez
G. Rosas
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: [email protected]
J. Chihuaque
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: [email protected]
E. Bedolla
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: [email protected]
R. Esparza
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Santiago de Querétaro, Qro., 76230, México.
R. Pérez
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Santiago de Querétaro, Qro., 76230, México.
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Abstract

In this investigation, the chemical and microstructural characteristics of nanostructured AlFe intermetallic produced by high-energy ball milling have been explored. High purity elemental powders were used as the starting material. The ball milling was carried out at room temperature using a SPEX-8000 mixer/mill. The structure, morphology and compositions of the powders were obtained using X-ray diffraction patterns (XRD), scanning and transmission electron microscopy (STEM). High resolution electron microscopy observations have been used in the nanostructured materials characterization. The structural configurations have been explored through comparisons between experimental HREM images and theoretically simulated images obtained with the multislice method of the dynamical theory of electron diffraction.

Keywords

NanostructureAlScanning Electron Microscopy (SEM)Transmission Electron Microscopy (TEM)X-ray diffraction (XRD)
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1766: Symposium 5B – Structural and Chemical Characterization of Metals, Alloys, and Compounds—2014 , 2015 , pp. 181 - 186
Copyright
Copyright © Materials Research Society 2015 

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References

REFERENCES

Moriarty, P., Rep. Prog. Phys., 64, 297 (2001).CrossRefGoogle Scholar
Guihen, E., Glennon, J. D., Analytical Letters, 36, 3309 (2003).CrossRefGoogle Scholar
Mamalis, A.G., Journal of Materials Processing Technology, 181, 52 (2007).CrossRefGoogle Scholar
Iijima, S., Ichihashi, T., Nature, 363, 603 (1993).CrossRefGoogle Scholar
Hu, X., Cheng, W., Wang, T., Wang, E., Dong, S., Nanotechnology, 16, 2164 (2005).CrossRefGoogle Scholar
Wang, Y., Kim, M.J., Shan, H., Kittrell, C., Fan, H., Ericson, L.M., Hwang, W., Arepalli, S., Hauge, R.H., Smalley, R.E., Nano Lett., 5, 997 (2005).CrossRefGoogle Scholar
Panigrahi, S., Kundu, S., Ghosh, S. K., Nath, S., Pal, T., Journal of Nanoparticle Research, 6, 411 (2004).CrossRefGoogle Scholar
Esparza, R., Ascencio, J.A., Rosas, G., Sánchez Ramírez, J.F., Pal, U., Perez, R., Journal of Nanoscience and Nanotechnology, 5, 641 (2005).CrossRefGoogle Scholar
Daniel, M.C., Astruc, D., Chem. Rev., 104, 293 (2004).CrossRefGoogle Scholar
Beyer, M.K., Clausen Schaumann, H., Chem. Rev., 105, 2921 (2005).CrossRefGoogle Scholar
Suryanarayana, C., Prog. Mater. Sci, 46, 1 (2001).CrossRefGoogle Scholar
Wieczorek Ciurowa, K., Gamrat, K., Journal of Thermal Analysis and Calorimetry, 88, 213 (2007).CrossRefGoogle Scholar
Rosas, G., Sistos, J., Ascencio, J.A., Medina, A., Pérez, R., Appl. Phys. A, 80, 377 (2005).CrossRefGoogle Scholar
Ayala-Sistos, J., Rosas, G., Esparza, R., Pérez, R., Adv. in Tech. of Mat. and Mat. Proc. J. (ATM) , 7, 175 (2005).Google Scholar
Kouravelou, K.B., Sotirchos, S.V., Rev. Adv. Mater. Sci. , 10, 243 (2005).Google Scholar
Zhao, Q.Q., Boxman, A., Chowdhry, U. , Journal of Nanoparticle Research , 5, 567 (2003).CrossRefGoogle Scholar
Schmid, G. , Nanoscale materials in chemistry , John Wiley & Sons, (2001).Google Scholar
Rellinghaus, B., Stappert, S., Acet, M., Wassermann, E.F., Journal of Magnetism and Magnetic Materials , 162, 142 (2003).CrossRefGoogle Scholar
Stappert, S., Rellinghaus, B., Acet, M., Wasseramann, E.F., The European Physical Journal D , 24, 351 (2003).CrossRefGoogle Scholar