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Synthesis and Texture of Mesophase Templated Silica Layers Seeded with Nanoparticles

Published online by Cambridge University Press:  10 February 2011

M. Klotz ,
A. Ayral ,
A. Van Der Lee ,
C. Guizard ,
C. MÉnager  and
V. Cabuil
M. Klotz
Affiliation:
Laboratoire des Matériaux et Procédés Membranaires UMR CNRS 5635, ENSCM, Montpellier (France)
A. Ayral
Affiliation:
Laboratoire des Matériaux et Procédés Membranaires UMR CNRS 5635, ENSCM, Montpellier (France)
A. Van Der Lee
Affiliation:
Laboratoire des Matériaux et Procédés Membranaires UMR CNRS 5635, ENSCM, Montpellier (France)
C. Guizard
Affiliation:
Laboratoire des Matériaux et Procédés Membranaires UMR CNRS 5635, ENSCM, Montpellier (France)
C. MÉnager
Affiliation:
Laboratoire de Physico-Chimie Inorganique, URA CNRS 430, Université P. et M. Curie, Paris (France)
V. Cabuil
Affiliation:
Laboratoire de Physico-Chimie Inorganique, URA CNRS 430, Université P. et M. Curie, Paris (France)
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Abstract

Mesophase templated silica layers seeded with magnetic or non magnetic nanoparticles are prepared. The study of the interactions between the nanoparticles and the others compounds of the synthesis solution is first described to explain the synthesis conditions allowing a homogeneous seeding. X-ray diffraction measurements are then used to study the texture of thick layers seeded with magnetic nanoparticles.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 576: Symposium DD – Organic/Inorganic Hybrid Materials II , 1999 , 247
Copyright
Copyright © Materials Research Society 1999

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References

REFERENCES

1. Kresge, C. T., Leonowicz, M. E., Roth, W. J., Vartuli, J. C. and Beck, J. S., Nature 359, 710 (1992).10.1038/359710a0Google Scholar
2. Beck, J. S., Vartuli, J. C., Roth, W. J., Leonowicz, M. E., Kresge, C. T., Schmitt, K. D., Chu, C. T. W., Olson, D. H., Sheppard, E. W., McCullen, S. B., Higgins, J. B. and Schenker, J. L., J. Am. Chem. Soc. 114, 10834 (1992).10.1021/ja00053a020Google Scholar
3. Monnier, A., Schüth, F., Huo, Q., Kumar, D., Margolese, D., Maxwell, R. S., Stucky, G. D., Krishnamurty, M., Petroff, P., Firouzi, A., Janicke, M. and Chmelka, B. F., Science 261, 1299 (1993).10.1126/science.261.5126.1299Google Scholar
4. Martin, J. E., Anderson, M. T., Odinek, J. and Newcomer, P., Langmuir 13, 4133 (1997).10.1021/la960714gGoogle Scholar
5. Dabadie, T., Ayral, A., Guizard, C., Cot, L. and Lacan, P., J. Mat. Chem. 6, 1789 (1996).10.1039/JM9960601789Google Scholar
6. Yang, H., Kuperman, A., Coombs, N., Mamiche-Afara, S. and Ozin, G. A., Nature 379, 703 (1996).10.1038/379703a0Google Scholar
7. Yang, H., Coombs, N., Sokolov, I. and Ozin, G. A., Nature 381, 589 (1996).10.1038/381589a0Google Scholar
8. Yang, H., Coombs, N., Sokolov, I. and Ozin, G. A., J. Mat. Chem. 7, 1285 (1997).10.1039/a608171aGoogle Scholar
9. Raimondi, M. E., Maschmeyer, T., Templer, R. H. and Seddon, J. M., Chem. Commun. 1843 (1997).Google Scholar
10. Liu, J., Kim, A. Y., Virden, J. W. and Bunker, B. C., Langmuir 11, 659 (1995).Google Scholar
11. Fabre, P., Casagrande, C., Veyssie, M., Cabuil, V. and Massart, R., Phys. Rev. Letters 64, 539 (1990).10.1103/PhysRevLett.64.539Google Scholar
12. Tolbert, S. H., Firouzi, A., Stucky, G. D. and Chmelka, B. F., Science 278, 264 (1997).10.1126/science.278.5336.264Google Scholar
13. Firouzi, A., Schaefer, D. J., Tolbert, S. H., Stucky, G. D. and Chmelka, B. F., J. Am. Chem. Soc. 119, 9466 (1997).10.1021/ja971267+Google Scholar
14. Van OS, N. M., Haak, J. R. and Rupert, L. A. M., Physico-chemical properties of selected anionic, cationic and nonionic surfactants (Elsevier, Amsterdam, 1993), p. 109.10.1016/B978-0-444-89691-9.50008-1Google Scholar
15. Massart, R., IEEE Trans. Magn. on Magn. Mag. 17, 1247 (1981).10.1109/TMAG.1981.1061188Google Scholar
16. Iler, R. K., The chemistry of silica (J. Wiley, New York, 1979) p. 388.Google Scholar