Hostname: page-component-cd9895bd7-p9bg8 Total loading time: 0 Render date: 2024-12-27T02:31:01.039Z Has data issue: false hasContentIssue false

Synthesis and Characterization of Nanoparticles of TiO2

Published online by Cambridge University Press:  01 February 2011

Rosa M. Lima García
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Juriquilla, Querétaro 76230, México
Rafael Quintero-Torres
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Juriquilla, Querétaro 76230, México
Get access

Abstract

The first steps in the synthesis of nanostructures are followed through UV-Vis and correlated with photoluminescence and images taken by SEM and TEM. Colloids permit the control in the atomic arrangement and the formation of nanostructures used to build cluster of materials. The size of the cluster in the colloid is around 5 nm. After the formation of the colloid a hydrothermal growth and microwave heating allows the formation of an ensemble of nano-sheet. This work is aim in the direction to controls the synthesis and the properties of materials with potential applications as active optical materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 2010

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Mashid, S., Askari, M., Sasani, M., Journal of Materials Processing Technology 189, 296 (2007).Google Scholar
2. Oskam, G., Nellore, A., Lee Penn, R., and Searson, P. C., J. Phys. Chem. B 107, 1734 (2003)Google Scholar
3. Osada, M., Ebina, Y., Funakubo, H., Yokoyama, S., Kiguchi, T., Takado, K., Sasaki, T., Advanced Materials 18, 1023 (2006)Google Scholar
4. Wang, Y. and Heron, N., J. Phys. Chem. 95, 525 (1991).Google Scholar
5. Mahshid, S., Sasani Ghamsari, M., Askari, M., Afshar, N., Lauthi, S., Semiconductor Physics, Quantum Electronics & Optoelectronics 9, 65 (2006).Google Scholar
6. Bischoff, Brian L. and Anderson, Marc A., Chemistry of Materials 7, 1772 (1995).Google Scholar
7. Wang, Y., Suna, A., Mahler, W. and Kasowski, R., J. Chem. Phys. 87, 7315 (1987).Google Scholar
8. Xu, Jiaoxing, Li, Liping, Yan, Youjun, Wang, Hui, Wang, Xuxu, Fu, Xianzhi, Li, Guangshe, Journal of Colloid and Interface Science 318, 29 (2008).Google Scholar
9. Pankove, J.I., Optical Processes in Semiconductors (1971).Google Scholar
10. Wilson, Gregory J., Will, Geoffrey D., Frost, Ray L. and Montgomery, Simon A., Journal of Materials Chemistry 12, 1781 (2002).Google Scholar
11. Beunsen, J., Van Bael, M. K., Van den Rul, H., Haen, J. D., Mullens, J., Journal of the European Ceramic Society 27, 4529 (2007).Google Scholar