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Quantitative Analysis of Segregation to Grain Boundaries in Steels

Published online by Cambridge University Press:  10 February 2011

A. J. Garratt-Reed
Affiliation:
Center for Materials Science and Technology, Massachusetts Institute of Technology, Cambridge, MA 02139–4307, U. S. A. Manchester Materials Science Centre, Grosvenor Street, Manchester Ml 7HS, U.K.
G. Cliff
Affiliation:
Manchester Materials Science Centre, Grosvenor Street, Manchester Ml 7HS, U.K.
G. W. Lorimer
Affiliation:
Manchester Materials Science Centre, Grosvenor Street, Manchester Ml 7HS, U.K.
R. Pilkington
Affiliation:
Manchester Materials Science Centre, Grosvenor Street, Manchester Ml 7HS, U.K.
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Abstract

Grain boundary segregation of phosphorous in model reactor steels has been measured using EDX Spectroscopy in the FEG-STEM. The results have been compared with Auger spectroscopy measurements made on similar materials. The results were in excellent agreement.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

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References

REFERENCES

1. Mitamura, T., Hall, E. L., Kingery, W. D. and Vander Sande, J. B., Ceramurgia Int. 5, 131136, 1979 Google Scholar
2. Ikeda, J. A. S., Chiang, Y-M., Garratt-Reed, A. J. and Vander Sande, J. B., J. Am. Ceram. Soc. 76, 24472459, 1993 Google Scholar
3. AGarratt-Reed, J., Proc. 50th. Ann. Mtg. EMSA, (San Francisco Press) 12061207, 1992 Google Scholar
4. Lee, J.-R., Chiang, Y.-M. and Ceder, G., Acta Mater. 45, 12471257, 1997 Google Scholar
5. Aoki, M., Chiang, Y.-M., Kosacki, I., Lee, L. J.-R., Tuller, H. and Liu, Y., J. Am. Ceram. Soc. 79, 11691180, 1996 Google Scholar
6. Terwilliger, C. D. and Chiang, Y.-M., Acta Metall. Mater. 43, 319328, 1995 Google Scholar
7. Chiang, Y.-M., Silverman, L. A., French, R. H. and Cannon, R. M., J. Am. Ceram. Soc. 77, 11431152, 1994 Google Scholar
8. Pilkington, R., Dicken, R., Peura, P., Lorimer, G. W., Allen, G. C., Holt, M. and Younes, C. M., Mater. Sci. & Eng. A212, 191205, 1996 Google Scholar
9. Cliff, G. and Lorimer, G. W., J. Microsc. 103, 203207, 1975 Google Scholar
10. Garratt-Reed, A. J. and Furdanowicz, W., Analytical Electron Microscopy, Ed. Joy, D. C. (San Francisco Press) 225227, 1987 Google Scholar
11. Hunt, C. P. and Seah, M. P., Mater. Sci. & Technol, 8, 10231035, 1992 Google Scholar