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Preparation of TEM Specimens of Rubber Modified Polymeric Materials by Ultramicrotomy and OsO4 Staining

Published online by Cambridge University Press:  16 February 2011

S. Yegnasubramanian
S. Yegnasubramanian*
Affiliation:
AT&T Bell Laboratories, Princeton, New Jersey 08540
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Abstract

This paper presents the specimen preparation approaches developed to image rubber(butadiene) - modified epoxy polymeric materials used in the microelectronics industry by TEM. The methodology is complicated by the fact that silica and calcium carbonate (>75 wt%) are used as filler materials while the rubber is used as a toughening agent in the samples investigated.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 199: Symposium W – Specimen Preparation for Transmission Electron Microscopy of Materials II , 1990 , 217
Copyright
Copyright © Materials Research Society 1990

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References

REFERENCES

[1] Kato, K., J. Electron Micros. 14, 220 (1965); Polymer Letters 4, 35, (1966).Google Scholar
[2] Gebizlioglu, O.S., Argon, A. S. and Cohen, R. E. in Specimen Preparation for Transmission Electron Microscopy of Materials edited by John Bravman, C., Anderson, Ron M., McDonald, Michael L. (Mater. Res. Soc. Proc. 115, Pittsburgh, PA 1987) pp. 137–142.Google Scholar
[3] Kramer, Vivian and Reimschuessel, Annemarie, in Proc. 46th Annual Meeting of the Electron Microscopy Society of America edited by Bailey, G. W., Milwaukee, Wisconsin, 1988, p. 930.Google Scholar
[4] Kruse, R. L., J. Micros. 123, 323 (1981).Google Scholar
[5] Masahiro Kakugo, Sadatoshi, H., Yokoyama, M., Kojima, K., Macromolecules, 22(2), 547 (1989)Google Scholar
[6] Froehling, P. E., Pijpers, A. J. J. Polym. Sci., Part B: Polym. Phys., 25(4), 947 (1987)Google Scholar