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Preparation of amorphous aluminium ammonium phosphates

Published online by Cambridge University Press:  16 February 2012

Barbara Grzmil
Affiliation:
West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, 70-322 Szczecin, Pułaskiego 10, E-mail: [email protected]
Kinga Łuczka
Affiliation:
West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, 70-322 Szczecin, Pułaskiego 10, E-mail: [email protected]
Marta Gleń
Affiliation:
West Pomeranian University of Technology, Szczecin, Institute of Chemical and Environment Engineering, 70-322 Szczecin, Pułaskiego 10, E-mail: [email protected]
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Abstract

A method for obtaining of amorphous aluminium ammonium phosphates is developed. The statistical program STATISTICA 9 is used for planning and evaluation of the experiments. Research is carried out according to the Box-Behnken model for the following values of independent variables (input factors): pH: 6.0 ± 2; concentration of reagents: 40 ± 10 wt%, molar ratio of NH4+:PO43- in substrates (2 ± 1:1) i.e. Al3+:NH4+:PO43- (0.66:1-3:1). On the basis of this research, process parameters are determined, in which materials with the expected physicochemical properties (chemical composition, specific surface area, oil absorption number) can be obtained.

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Articles
Copyright
Copyright © Materials Research Society 2012

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References

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