Hostname: page-component-586b7cd67f-r5fsc Total loading time: 0 Render date: 2024-11-25T17:30:59.817Z Has data issue: false hasContentIssue false

Plastic Deformation and Recrystallization Studied by the 3-D x-ray Microscope

Published online by Cambridge University Press:  10 February 2011

D. Juul Jensen
Affiliation:
Materials Research Department, RisØ National Laboratory, Frederiksborgvej 399, DK-4000 Roskilde, Denmark
Å. Kvick
Affiliation:
ESRF, BP 220, F-38043 Grenoble Cedex, France
E.M. Lauridsen
Affiliation:
Materials Research Department, RisØ National Laboratory, Frederiksborgvej 399, DK-4000 Roskilde, Denmark
U. Lienert
Affiliation:
ESRF, BP 220, F-38043 Grenoble Cedex, France
L. Margulies
Affiliation:
Materials Research Department, RisØ National Laboratory, Frederiksborgvej 399, DK-4000 Roskilde, Denmark ESRF, BP 220, F-38043 Grenoble Cedex, France
S.F. Nielsen
Affiliation:
Materials Research Department, RisØ National Laboratory, Frederiksborgvej 399, DK-4000 Roskilde, Denmark
H.F. Poulsen
Affiliation:
Materials Research Department, RisØ National Laboratory, Frederiksborgvej 399, DK-4000 Roskilde, Denmark
Get access

Abstract

A newly developed synchrotron instrument – the so-called 3D X-ray microscope – is presented. The instrument is placed at the Materials Science beamline at ESRF and dedicated to local μm scale structural characterization within bulk materials. In this paper, emphasis is on in situ studies of thermomechanical processing. The potential of the instrument for characterization of single nuclei and grains is described and discussed based on both first results and planned experiments.

Type
Research Article
Copyright
Copyright © Materials Research Society 2000

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Proceedings of 4th Int. Conf. on Recrystallization and Related Phenomena, edited by Sakai, T. and Suzuki, H.G. (The Japan Inst. of Metals, Sendai, Japan, 1999).Google Scholar
2. Proceedings of 20th Risø Int. Symp. on Materials Science, Deformation-Induced Microstructures: Analysis and Relation to Properties, edited by Bilde-Sørensen, J.B. et al. (Risø Nat. Lab., Roskilde, Denmark, 1999).Google Scholar
3. Proceedings 3rd Int. Conf. on Grain Growth in Polycrystalline Materials, edited by Weiland, H., Adams, B.L. and Rollett, A.D. (The Minerals, Metals and Materials Society, 1998).Google Scholar
4. Hansen, N. and Jensen, D. Juul, Phil. Trans. R. Soc. London 357, p. 1447, 1467 (1999).10.1098/rsta.1999.0384Google Scholar
5. Poulsen, H.F., Garbe, S., Lorentzen, T., Jensen, D. Juul, Poulsen, F.W., Andersen, N.H., Frello, T., Feidenhans'l, R., Graafsma, H., J. Synchrotron Rad. 4, p. 147154 (1997).10.1107/S0909049597002021Google Scholar
6. Lienert, U., Poulsen, H.F. and Kvick, Å. in Proceedings of the 40th Conference of the American Institute of Aeronautics and Astronautics on Structures, Structural Dynamics and Materials (St. Louis, USA, 1999) A99-24795, p. 20672075.Google Scholar
7. Lienert, U., Martins, R., Grigull, S., Pinkerton, M., Poulsen, H.F., Kvick, Å., these proceedings.Google Scholar
8. Lienert, U., Schulze, C., Honkimäki, V., Tschentscher, T., Garbe, S.. Hignette, O., Horsewell, A., Lingham, M., Poulsen, H.F., Thomsen, N.B., Ziegler, E., J. Synchrotron Rad. 5, p. 226, 231 (1998).10.1107/S0909049598001393Google Scholar
9. Poulsen, H.F., Nielsen, S.F., Lauridsen, E.M., Lienert, U., Suter, R.M. and Jensen, D. Juul. Submitted for publication.Google Scholar
10. Nielsen, S.F., Wolf, A., Poulsen, H.F., Ohler, M., Lienert, U. and Owen, R.A., in print J. Synchrotron Rad. Google Scholar
11. Lienert, U., Poulsen, H.F., Honkimäki, V., Schulze, C., Hignette, O., J. Synchrotron Rad. 9, p. 979, 984, (1999).10.1107/S0909049599001934Google Scholar
12. Proceedings 6th Conf. on Frontiers of Electron Microscopy in Materials Science, Ultramicroscopy 67 (1997).Google Scholar
13. Watanabe, T. in Proc. Textures of Materials ICOTOM 11, edited by Liang, Z. et al. (Int. Academic Publishers, Beijing 1996) p. 13091318.Google Scholar
14. Palumbo, G., King, P.J., Aust, K.T., Erb, U. and Lichtenberger, I.c., Scripta metall. mater. 25, p. 1775, 1780 (1991).10.1016/0956-716X(91)90303-IGoogle Scholar
15. Lin, P., Palumbo, G., Erb, U. and Aust, K.T., Scripta metall. mater. 33, p. 1387, 1392 (1995).10.1016/0956-716X(95)00420-ZGoogle Scholar
16. Palumbo, G. and Aust, K.T. in Proc. Grain Growth in Polycrystalline Materials III, edited by Weiland, H. et al. (The Minerals, Metals & Materials Society, 1998) pp. 311320.Google Scholar
17. Adams, B.L. and Wu, C.T. in Proc. Textures of Materials ICOTOM 11, edited by Liang, Z. et al. , Int. Academic Publishers, Beijing, 1996, pp. 2330.Google Scholar
18. Lassen, N.C. Krieger, Jensen, D. Juul and Conradsen, K., Scan. Microscopy 6, p. 115, 121 (1992).Google Scholar
19. Wright, S.I. and Adams, B.L., Metall. Trans. 23A, p. 759, 767 (1992).10.1007/BF02675553Google Scholar
20. Kral, M.V. and Spanos, G., Acta mater. 47, p. 711, 724 (1999).10.1016/S1359-6454(98)00321-8Google Scholar
21. Rollett, A.D. et al. in Microscopy and Microanalysis, Springer, 1999, pp. 230231.Google Scholar
22. Huang, X. and Liu, Q., Ultramicroscopy 74, p. 123, 130 (1998)10.1016/S0304-3991(98)00033-3Google Scholar
23. Liu, Q., Ultra microscopy 60, p. 81, 89 (1995).10.1016/0304-3991(95)00049-7Google Scholar
24. Krieger, N.C. Lassen in Proc. 16th Risø Int. Symp. on Mat. Sci., edited by Hansen, N. et al. (Risø, Roskilde, Denmark, 1995), p. 405411.Google Scholar
25. Dingley, D.J., Scan. Electron Microscopy 11, p. 569, 575 (1984).Google Scholar
26. Huang, X. and Hansen, N., Scripta mater. 37, p. 1, 7 (1997).10.1016/S1359-6462(97)00072-9Google Scholar
27. Winther, G., Jensen, D. Juul and Hansen, N., Acta mater. 45, p. 5059, 5068 (1997).10.1016/S1359-6454(97)00168-7Google Scholar
28. Taylor, G.I., J. Inst. Met. 62, p. 307, 324 (1938).Google Scholar
29. Driver, J.H. in Proc. 16th Risø Int. Symp. on Mat. Sci. edited by Hansen, N. et al. (Risø, Roskilde, Denmark, 1995) p. 2536.Google Scholar
30. Godfrey, Ä., Jensen, D. Juul and Hansen, N., Acta mater. 46, p. 823, 833 and p. 835, 848 (1998).10.1016/S1359-6454(97)00315-7Google Scholar
31. Liu, Q. and Hansen, N., Proc. R. Soc. Lond. A454, p. 1, 19 (1998).Google Scholar
32. Weiland, H. and Hirsch, J.R., Textures and Microstructures 14–18, p. 647, 652 (1991).10.1155/TSM.14-18.647Google Scholar
33. Samajdar, I. and Doherty, R.D., Scripta metall. mater. 32, p. 845, 850 (1995).10.1016/0956-716X(95)93212-MGoogle Scholar
34. Vatne, H.E., Daaland, O. and Nes, E., Mat. Sci. Forum 157–162, p. 1087, 1094 (1994).10.4028/www.scientific.net/MSF.157-162.1087Google Scholar
35. Jensen, D. Juul, Acta mater. 43, p. 4117, 4129 (1995).10.1016/0956-7151(95)00111-8Google Scholar
36. Cahn, J.W. and Hagel, W.C. in Decomposition of Austenite by Diffusional Processes, edited by Zackay, V.F. and Aaronson, H.I. (Interscience 1962), p. 131196.Google Scholar
37. Jensen, D. Juul, Scripta metall. mater. 27, p. 533538 (1992).10.1016/0956-716X(92)90335-CGoogle Scholar
38. Engler, O., Acta mater. 46, p. 1555, 1568 (1998).10.1016/S1359-6454(97)00354-6Google Scholar
39. Vandermeer, R.A. in Proc. 16th Risø Int. symp. on Mat. Sci., edited by Hansen, N. et al. (Risø, Roskilde, Denmark, 1995), p. 193213.Google Scholar
40. Vandermeer, R.A. and Jensen, D. Juul, Acta metall. mater. 42, p. 2427, 2436 (1994).10.1016/0956-7151(94)90321-2Google Scholar
41. Vandermeer, R.A. and Jensen, D. Juul, Met. Trans. A 26, p. 2227, 2235 (1995).10.1007/BF02671238Google Scholar
42. Lauridsen, E.M., Jensen, D. Juul, Lienert, U. and Poulsen, H.F., submitted for publication.Google Scholar