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Published online by Cambridge University Press: 17 March 2011
We have synthesized ZnMgO alloy of wurtzite (Mg content equals to 0.0=0.34) and cubic (Zn content equals to 0.0- 0.18) phases using nonequilibrium pulsed laser deposition method. Epitaxial films of ZnMgO wurtzite structure have been grown on (0001) sapphire substrates. Using JEOL-2010 field-emission transmission electron microscope equipped with STEM and Gatan image filter, we can perform atomic structure, STEM-Z, electron energy loss spectroscopy and imaging simultaneously. Such studies on the ZnO/MgZnO superlattices provide first direct evidence of phase-separation in the range 3 nm.