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Perspective on Submicron-Resolution Three-Dimensional X-Ray Structural Microscopy to Address Mesoscale Materials Microstructure and Evolution Issues

Published online by Cambridge University Press:  01 February 2011

B. C. Larson
Affiliation:
Condensed Matter Sciences Division, Oak Ridge National Laboratory Oak Ridge, TN 37831-6030, U.S.A.
Wenge Yang
Affiliation:
Condensed Matter Sciences Division, Oak Ridge National Laboratory Oak Ridge, TN 37831-6030, U.S.A. Guest Scientist; University of TN-Knoxville
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Abstract

This paper provides a perspective on submicron-resolution three-dimensional x-ray structural microscopy for the investigation of materials microstructure and evolution on mesoscopic length scales. Microstructure and thermal/stress induced microstructure evolution at the length scale of the local crystal grains, grain boundaries, triple junctions, and dislocation patterning are known to play critical roles in determining the physical properties of materials. Large scale computer simulations and multi-scale modeling are making significant progress on the nanoscale and detailed mesoscale computations are becoming increasingly tractable as new methods are developed. X-ray structural microscopy with submicron resolution now provides a (previously missing) direct experimental link between theory and computations and the mesoscopic behavior of materials microstructure.

Type
Research Article
Copyright
Copyright © Materials Research Society 2005

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References

1 Sherby, O.D. and Wadsworth, J., Scientific American 252, (1985).Google Scholar
2 Verhoeven, J., Scientific American 284, 62 (2001).Google Scholar
3 Needleman, A., Acta Mater. 48, 105 (2000).Google Scholar
4 Derlet, P.M., Petegem, S. Van, and Swygenhoven, H. Van, Phys. Rev. B 71, 024114 (2005).Google Scholar
5 Wolf, D., Yamakov, V., Phillpot, S.R., Mukherjee, A., and Gleiter, H., Acta Mater. 53, 1 (2005).Google Scholar
6 El-Azab, A., Phys. Rev. B 61, 11956 (2000).Google Scholar
7 Humphreys, F.J., J. Mat. Sci. 36 3833 (2001).Google Scholar
8 Wilkinson, A.J. and Hirsch, P.B., Micron 28, 279 (1997).Google Scholar
9 Larson, B. C. and Lengeler, B., MRS Bulletin 29, 152 (2004).Google Scholar
10 Poulsen, H.F., Jensen, D.J., and Vaughan, G.B.M., MRS Bulletin 29, 166 (2004).Google Scholar
11 Ice, G.E. and Larson, B.C., MRS Bulletin 29, 170 (2004).Google Scholar
12 Poulsen, H.F., Three-Dimensional X-Ray Diffraction Microscopy – Mapping Polycrystals and Their Dynamics, (Springer-Verlag Berlin, Berlin 2004).Google Scholar
13 Poulsen, H.F., Fu, X, Knudsen, E., Lauridsen, E.M., Margulies, L., and Schmidt, S., Materials Science Forum, 467-470, 1363 (2004).Google Scholar
14 Fu, X., Poulsen, H.F., Schmidt, S., Nielsen, S. F., Lauridsen, E.M., and Jensen, D.J., Scripta Mater. 49, 1093 (2003).Google Scholar
15 Larson, B.C., Yang, W., Ice, G.E., Budai, J.D., and Tischler, J.Z., Nature 415, 887 (2002).Google Scholar
16 Schmidt, S., Nielsen, S.F., Gundlach, C., Margulies, L., Huang, X., and Jensen, D.J., Science 305, 229 (2004).Google Scholar
17 Yang, W., Larson, B.C., Tischler, J.Z., Ice, G.E., Budai, J.D., and Liu, W., Micron 35, 431 (2004).Google Scholar
18 Budai, J.D., Yang, W., Larson, B.C., Tischler, J.Z., Liu, W., Weiland, H., and Ice, G.E., Materials Science Forum, 467-470, 1373 (2004).Google Scholar
19 Yang, W., Larson, B.C., Ice, G.E., Tischler, J.Z., Budai, J.D., JChung, .S., and Lowe, W.P., Appl. Phys. Lett. 82, 3856 (2003).Google Scholar
20 Larson, B.C., Yang, W., tischler, J.Z., Ice, G.E., budai, J.D., Liu, W., and Weiland, H., Int. J. Plasticity 20, 543 (2004).Google Scholar
21 Hughes, D.A. and Hansen, N., Acta Mater 45, 3871 (1997).Google Scholar
22 Yang, W., Larson, B.C., Pharr, G.M., Budai, J.D., Tischler, J.Z., and Liu, W., J. Mater. Res. 19, 66 (2004).Google Scholar