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A Novel Sample Design for Easier X-Tem Specimen Preparation of Surface Coated Hardened High Speed Steel

Published online by Cambridge University Press:  10 February 2011

Klaus F. Østergaard  and
K. A. Mørch
Klaus F. Østergaard
Affiliation:
Department of Physics, Technical University of Denmark, DK-2800 Lyngby, Denmark, [email protected] and [email protected]
K. A. Mørch
Affiliation:
Department of Physics, Technical University of Denmark, DK-2800 Lyngby, Denmark, [email protected] and [email protected]
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Abstract

A novel design of test sample for X-TEM specimen preparation is presented. The test sample is particurlarly suited for surface coatings on hardened steel (heat treated materials). The technique for cutting and preparation of a specimen from the test sample is given in some detail and a few hints about ion thinning and X-TEM analysis are included.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 480: Symposium Z – Specimen Preparation for Transmission Electron Microscopy…IV , 1997 , 97
Copyright
Copyright © Materials Research Society 1997

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References

1. Østergaard, K.F., Initial Growth of Titanium Nitride on M2 High Speed Steel - The Development and Implementation of Techniques and Facilities to Produce and Study the Initial Layer of CVD TiN on High Speed Steel. M.Sc. Thesis, Dept. of Physics, Tech. Univ. Denmark 1996.Google Scholar
2. Barna, Á. in Specimen Preparation for Transmission Electron Microscopy of Materials - III, edited by Anderson, R., Tracy, B. and Bravman, J. (Mat.Res.Soc. Symp. 254, Boston, Ma. 1991) p. 3–22.Google Scholar
3. Hardened cutting tools supplied by Technoorg Linda, Rózsa u. 24, Budapest, H-1077, Hungary, Phone +36 361 342 8713.Google Scholar
4. J.P., McCaffrey, A., Barna Accepted Microscopy Research & Technique.Google Scholar
5. The alumina ring is obtainable from companies that sell lasered ceramics to the hybrid microelectronic industry. E.g. Laser Technical Services A/S, Sneppevang 3, DK-3450 Allerød, Denmark, Tel: +45 48 17 61 61, Fax: +45 48 17 10 65.Google Scholar