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Microstructure and Strengthening of Creep-Tested Cryomilled NiAl-AlN

Published online by Cambridge University Press:  15 February 2011

Anita Garg
Affiliation:
AYT/NASA Lewis Research Center, 21000 Brookpark Rd., Cleveland, OH 44135
J. Daniel Whittenberger
Affiliation:
AYT/Exxon Research and Engineering Company, Rt. 22 East Annandale, NJ 08801
Michael J. Luton
Affiliation:
AYT/Exxon Research and Engineering Company, Rt. 22 East Annandale, NJ 08801
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Abstract

The mechanical grinding of prealloyed NiAl powder in liquid nitrogen (cryomilling) results in an intermetallic matrix composite where micron sized particle free aluminide cores (grains) are surrounded by thin mantles comprised of nanometer sized A1N particles and NiAl grains. Under high temperature, slow strain rate conditions both compressive and tensile creep testing have shown that the mechanical strength of hot extruded cryomilled NiAl approaches the levels exhibited by advanced NiAl-based single crystals and simple Ni-based superalloys. Transmission electron microscopy of cryomilled materials tested between 1100 and 1300 K revealed little, if any, dislocation structure within the mantle regions, while the NiAl cores contained subgrains and dislocation networks after testing at all strain rates between 10-4 and 10-8 s-1. These and other microstructural observations suggest that creep strength is the result of a fine NiAl grain/subgrain size, the inability of dislocations to move through the mantle and stabilization of the microstracture by the A1N particles.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

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References

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