Hostname: page-component-586b7cd67f-vdxz6 Total loading time: 0 Render date: 2024-11-25T17:43:36.659Z Has data issue: false hasContentIssue false

Measurement of the Fracture Energy of SiO2/TiN Interfaces Using the Residually-Stressed Thin-Film Micro-Strip Test

Published online by Cambridge University Press:  10 February 2011

Guanghai Xu
Affiliation:
Materials Department, University of California, Santa Barbara, CA 93106
D. D. Ragan
Affiliation:
Materials Department, University of California, Santa Barbara, CA 93106
D. R. Clarke
Affiliation:
Materials Department, University of California, Santa Barbara, CA 93106
Ming Y. He
Affiliation:
Materials Department, University of California, Santa Barbara, CA 93106
Qing Ma
Affiliation:
Intel Corporation, Santa Clara, CA 95054
H. Fujimoto
Affiliation:
Intel Corporation, Santa Clara, CA 95054
Get access

Abstract

One of the key factors affecting the long-term reliability of thin film structures in microelectronics devices is the fracture resistance of their interfaces. Of the many different interfaces formed during device fabrication, the SiO2/TiN interface is amongst the most common. In order to measure the fracture energy of this interface, we have been utilizing a test in which a narrow strip of a material, having a large intrinsic tensile stress, is deposited and lithographically defined onto the SiO2/TiN/Al thin film structure. The elastic strain energy in the micro-strip provides an additional driving force to debond the weakest interface in the structure. Decohesion occurs when the thickness of the micro-strip, and hence the total elastic strain energy, exceeds a critical value. Another measure of the fracture resistance in the same test is the length of the strip that remains intact after debonding at both ends. This is a function of the intrinsic stress, the thickness of the superlayer, and the modulus ratios. In addition to presenting results on the measured fracture energy of the SiO2/TiN interface, evidence for stress-corrosion will be described.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Hutchinson, J.W., and Suo, Z., Mixed Mode Cracking in Layered Materials, Adv. Appl. Mech., 29, 63191, 1992 Google Scholar
2. Bagchi, A., Lucas, G.E., Suo, Z., and Evans, A.G., A New Procedure for Measure the Decohesion Energy of Thin Ductile Films on Substrates, J. Mater. Res., 9, 1734–41, 1994 Google Scholar
3. Gupta, V. and Pronin, A., J. Am. Ceram. Soc. 78 1397 (1995).Google Scholar
4. Suo, Z., and Hutchinson, J.W., Interface Crack between two Elastic Layers, Int. J. Fracture 43, 118, 1990 Google Scholar
5. Stoney, G.G., Proc. R. Soc. London Ser., vol. A 82, 172, 1909 Google Scholar